Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (8): 1261-1280.DOI: 10.1007/s40195-023-01544-5
Special Issue: 钛及钛合金
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Solomon Kerealme Yeshanew1,2, Chunguang Bai1(
), Qing Jia1, Tong Xi1, Zhiqiang Zhang1, Diaofeng Li1, Zhizhou Xia1,2, Rui Yang1, Ke Yang1(
)
Received:2022-10-09
Revised:2023-01-08
Accepted:2023-01-10
Online:2023-08-10
Published:2023-03-22
Contact:
Chunguang Bai cgbai@imr.ac.cn.Ke Yang kyang@imr.ac.cn
Solomon Kerealme Yeshanew, Chunguang Bai, Qing Jia, Tong Xi, Zhiqiang Zhang, Diaofeng Li, Zhizhou Xia, Rui Yang, Ke Yang. Influence of Hot-Rolling Deformation on Microstructure, Crystalline Orientation, and Texture Evolution of the Ti6Al4V-5Cu Alloy[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(8): 1261-1280.
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| Al | V | Cu | Fe | C | N | O | H | Ti |
|---|---|---|---|---|---|---|---|---|
| 6.13 | 4.18 | 5.65 | 0.17 | 0.011 | 0.007 | 0.10 | 0.002 | Bal. |
Table 1 Chemical composition of the as received Ti6Al4V- 5Cu alloy (wt%)
| Al | V | Cu | Fe | C | N | O | H | Ti |
|---|---|---|---|---|---|---|---|---|
| 6.13 | 4.18 | 5.65 | 0.17 | 0.011 | 0.007 | 0.10 | 0.002 | Bal. |
Fig. 3 a X-ray diffraction patterns of the Ti6Al4V-5Cu alloy after hot rolling, b magnified image of selected diffraction areas of a. The legend expressed the initial alloy for study (OI) and various thickness reduction ratios of 15%, 58%, and 73%
Fig. 4 a DSC curve of as cast Ti6Al4V-5Cu alloy, b OM observation of the heat-treated sample at 920 °C for 1 h, and exposed to slower air-cooling rate (AC), c SEM metallographic revealing the formation of kinked α lamellar structures and presence of β phase at 790 °C
Fig. 5 OM images demonstrating the effect of hot rolling deformation on microstructure evolution of the Ti6Al4V-5Cu alloy at TRR’s of: a 15%, b 58%, c 73%. EBSD images showing the grain structure in the alloy deformed at TRR’s of: d 15%, e 58%, f 73%
| No | Thickness reduction, TR (%) | Grain size (µm) | Phase volume fraction (%) | |||
|---|---|---|---|---|---|---|
| Min | Max | Average | α phase | β phase | ||
| 1 | 15 | 1.43 | 9.33 | 2.04 ± 1.46 | 90.8 | 9.2 |
| 2 | 58 | 1.43 | 12.3 | 1.88 ± 0.78 | 58.6 | 23.5 |
| 3 | 73 | 1.43 | 53.01 | 2.51 ± 2.1 | 98.3 | 1.7 |
Table 2 Average grain size of the microstructure and the average phase volume of the α and β of the hot rolled Ti6Al4V-5Cu alloy at various TRR’s
| No | Thickness reduction, TR (%) | Grain size (µm) | Phase volume fraction (%) | |||
|---|---|---|---|---|---|---|
| Min | Max | Average | α phase | β phase | ||
| 1 | 15 | 1.43 | 9.33 | 2.04 ± 1.46 | 90.8 | 9.2 |
| 2 | 58 | 1.43 | 12.3 | 1.88 ± 0.78 | 58.6 | 23.5 |
| 3 | 73 | 1.43 | 53.01 | 2.51 ± 2.1 | 98.3 | 1.7 |
Fig. 7 Relationship plot showing the influence of grain rotation on the texture fiber separation angle to maintain the BOR of {0001}α//{110}β on the 15% hot-rolled Ti6Al4V-5Cu alloy
Fig. 9 Relationship plot showing the influence of grain rotation on the α/β fiber texture interface separation angle between {0001}α and {110}β of the 58% hot rolled Ti6Al4V-5Cu alloy
Fig. 11 Relationship plot showing the influence of grain rotation on the α/β fiber texture separation angle between {0001}α and {110}β of the 73% hot rolled Ti6Al4V-5Cu alloy
Fig. 12 a High resolution TEM investigation showing that an activated prismatic and pyramidal slip planes along the [$\overline{2 }$ 4 $\overline{2 }$ 3], and Ti2Cu intermetallic compound, b basal, prismatic, and pyramidal slip plane in the [2 $\overline{1 }\overline{1 }$ 0] and [1 $\overline{2 }$ 1 $\overline{3 }$] slip directions observed on the 15% deformed sample
Fig. 13 a SADP using TEM at lower magnification, b the higher magnification of the portion, Pt.1, revealed that the Ti6Al4V-5Cu alloy after 58% thickness reduction was made up of α pyramidal plane along [01 $\overline{1 }$ 1] and, β of [$\overline{2 }$ 33] and [$\overline{1 }$ 23] slip directions c
Fig. 14 Selected high bright diffraction pattern using TEM investigation revealed that the Ti6Al4V-5Cu alloy after a 73% thickness reduction was made up of various activated slip planes
Fig. 15 Selected high bright fields of diffraction obtained using TEM investigation revealed that the 73% deformed Ti6Al4V-5Cu alloy was composed of slip planes of: α (hcp) pyramidal along the [$1\overline{2 }$ 1 $\overline{3 }$], [01 $\overline{1 }$ 2], and β of [$\overline{1 }$ 11], [$\overline{2 }$ 33], [01 $\overline{3 }$], and [113]
Fig. 16 Grain boundary misorientation angle distributions in the Ti6Al4V-5Cu alloy deformed at various thickness reduction ratios of: a 15%, b 58%, c 73%. The peaks at 65$^\circ$ and 85$^\circ$ correspond to {11 $\overline{2 }$ 2} < 11 $\overline{2 }\overline{3 }$> compressive twins and {10 $\overline{1 }$ 2} < 10 $\overline{1 }\overline{1 }$> tensile twins, respectively
| No | TR (%) | Grain size (µm) | Phase volume (%) | Yield strength,YS (MPa) | Ultimate tensile strength, UTS (MPa) | Tensile elongation, El (%) | Vickers hardness (kgf/mm2) | |||
|---|---|---|---|---|---|---|---|---|---|---|
| Min | Max | Average | α phase | β phase | ||||||
| 1 | 15 | 1.43 | 9.33 | 2.04 ± 1.46 | 90.8 | 9.2 | 1106 | 1267 | 13.01 | 405.4 |
| 2 | 58 | 1.43 | 12.3 | 1.88 ± 0.78 | 58.6 | 23.5 | 937.33 | 1188.67 | 23.15 | 418.8 |
| 3 | 73 | 1.43 | 53.01 | 2.51 ± 2.1 | 98.3 | 1.7 | 831.33 | 1221 | 19.73 | 397.8 |
Table 3 Mean grain size, α/β phase fraction and tensile property of the Ti6Al4V-5Cu alloy under different TRR’s
| No | TR (%) | Grain size (µm) | Phase volume (%) | Yield strength,YS (MPa) | Ultimate tensile strength, UTS (MPa) | Tensile elongation, El (%) | Vickers hardness (kgf/mm2) | |||
|---|---|---|---|---|---|---|---|---|---|---|
| Min | Max | Average | α phase | β phase | ||||||
| 1 | 15 | 1.43 | 9.33 | 2.04 ± 1.46 | 90.8 | 9.2 | 1106 | 1267 | 13.01 | 405.4 |
| 2 | 58 | 1.43 | 12.3 | 1.88 ± 0.78 | 58.6 | 23.5 | 937.33 | 1188.67 | 23.15 | 418.8 |
| 3 | 73 | 1.43 | 53.01 | 2.51 ± 2.1 | 98.3 | 1.7 | 831.33 | 1221 | 19.73 | 397.8 |
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