Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (4): 623-636.DOI: 10.1007/s40195-022-01498-0
Special Issue: 钢铁-2 2023; 焊接 2023
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Xuelin Wang1,2(
), Wenjuan Su1, Zhenjia Xie1, Xiucheng Li1, Wenhao Zhou3, Chengjia Shang1,2(
), Qichen Wang4,5, Jian Bai4,5, Lianquan Wu6
Received:2022-08-15
Revised:2022-09-09
Accepted:2022-09-22
Online:2023-04-10
Published:2023-03-31
Contact:
Xuelin Wang, xuelin2076@ustb.edu.cn; Chengjia Shang, cjshang@ustb.edu.cn
Xuelin Wang, Wenjuan Su, Zhenjia Xie, Xiucheng Li, Wenhao Zhou, Chengjia Shang, Qichen Wang, Jian Bai, Lianquan Wu. Microstructure Evolution of Heat-Affected Zone in Submerged Arc Welding and Laser Hybrid Welding of 690 MPa High Strength Steel and its Relationship with Ductile-Brittle Transition Temperature[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(4): 623-636.
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| Material | C | Si | Mn | P | S | Cr | Nb | V | Ti | Ni | Cu | Mo | B | Alt |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Experimental steel | 0.08 | 0.3 | 1.55 | 0.008 | 0.002 | 0.32 | 0.04 | 0.035 | 0.015 | - | - | 0.016 | 0.0016 | 0.04 |
| SAW welding wire | 0.08 | 0.05 | 1.53 | 0.013 | 0.001 | 0.018 | - | - | - | 0.01 | 0.02 | - | - | - |
| LHW welding wire | 0.07 | 0.8 | 1.45 | 0.015 | 0.014 | - | - | - | - | - | 0.15 | - | - | - |
Table 1 Chemical compositions of the experimental steel and welding wires (wt%)
| Material | C | Si | Mn | P | S | Cr | Nb | V | Ti | Ni | Cu | Mo | B | Alt |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Experimental steel | 0.08 | 0.3 | 1.55 | 0.008 | 0.002 | 0.32 | 0.04 | 0.035 | 0.015 | - | - | 0.016 | 0.0016 | 0.04 |
| SAW welding wire | 0.08 | 0.05 | 1.53 | 0.013 | 0.001 | 0.018 | - | - | - | 0.01 | 0.02 | - | - | - |
| LHW welding wire | 0.07 | 0.8 | 1.45 | 0.015 | 0.014 | - | - | - | - | - | 0.15 | - | - | - |
| Welding method | Current (A) | Voltage (V) | Welding speed (cm/min) | Heat input (kJ/cm) | Welding wire | Diameter of welding wire (mm) |
|---|---|---|---|---|---|---|
| SAW | 501 | 34.1 | 30 | 34.2 | AWS A5.17 F7A0-EH14 | 4.0 |
| LHW | 280 | 25 | 100 | 4.2 | AWS A5.18 ER70S-6 | 1.2 |
Table 2 Welding process parameters
| Welding method | Current (A) | Voltage (V) | Welding speed (cm/min) | Heat input (kJ/cm) | Welding wire | Diameter of welding wire (mm) |
|---|---|---|---|---|---|---|
| SAW | 501 | 34.1 | 30 | 34.2 | AWS A5.17 F7A0-EH14 | 4.0 |
| LHW | 280 | 25 | 100 | 4.2 | AWS A5.18 ER70S-6 | 1.2 |
Fig. 1 Macro morphologies of the welded joints obtained by using SAW a and LHW b, and location of the measurement of mechanical properties in the test samples
Fig. 2 Impact toughness and DBTT evolution in welded zones of SAW and LHW: a-c impact toughness of WM, FL and HAZ at series temperature, d DBTT of WM, FL and HAZ
Fig. 6 Optical microstructure evolution in welded joints of SAW a-d and LHW e-h: a, e WM, b, f CGHAZ, c, g FGHAZ, and d, h ICHAZ. (AF: acicular ferrite, GBF: grain boundary ferrite, GB: granular bainite, LB: lath bainite, QPF: quasi-polygonal ferrite, BF: bainitic ferrite, M/A: matrensite/austenite constituent)
Fig. 7 BC maps showing the microstructure evolution in welded joints of SAW a-c and LHW d-f: a, d WM, b, e FGHAZ, and c, f ICHAZ. (RA: retained austenite)
Fig. 8 BC maps a, d, boundaries distribution maps b, e and IPF maps c, f showing CGHAZ microstructure evolution in welded joints of SAW a-c and LHW d-f
Fig. 9 Grain boundaries distribution a, and volume fraction and average size of retained austenite (RA, fcc phase) b obtained in CGHAZ of SAW and LHW joints
Fig. 10 IPF maps a,e showing prior austenite grains reconstructed in CGHAZ of SAW a-d and LHW joints e-h and the corresponding {100}bcc pole figures b, f with symbols and numbers indicating the ideal 24 variants, and {110}bcc c, g and {111}fcc d, h pole figures calibrated by theoretical variants for inner microstructure of prior austenite
Fig. 11 Gran boundaries distribution maps a, e, and CP b, f and Bain c, g group maps showing the crystallographic features in CGHAZ of SAW a-d and LHW e-h joints, and the corresponding transformation mechanisms d, h
Fig. 12 Fraction of 24 variants a and length of intervariant boundaries between V1 and other variants b in reconstructed austenite grains of CGHAZ. (Three colors are used to highlight the 24 variants that separately belong to three different Bain groups, corresponding to the Bain group maps in Fig. 9c and g
Fig. 13 In situ observation of the secondary cracks on the fractured V-notch Charpy sample of CGHAZ in SAW a-h and LHW i, j joints: a position of crack observation, b, c experimental and theoretical {100} pole figures of reconstructed austenite grains in Fig. 13d-f, d-f IPF maps of in situ reconstructed austenite grains, g-j grain boundaries distribution maps and Bain group maps of crack propagation
| Welding method | Size and proportion | WM | CGHAZ | FGHAZ | ICHAZ | BM | |||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| SAW | Structure size (μm) | PCG-W | 81.2 ± 11.4 | PAG | 42.7 ± 6.3 | PAG | - | PAG-W | 6.4 ± 2.5 | PAG-W | 6.4 ± 2.5 |
| AF | 2.1 ± 1.3 | Packet | 4.7 ± 3.2 | QPF | 4.6 ± 2.2 | QPF | 2.8 ± 1.5 | Packet | 11.2 ± 3.8 | ||
| GBF-W | 28.3 ± 13.5 | Block | 7.7 ± 5.4 | M/A | 1.8 ± 0.7 | M/A | 1.6 ± 0.6 | Block | 2.4 ± 0.5 | ||
| RA | 0.8 ± 0.3 | RA | 0.8 ± 0.2 | RA | 0.4 ± 0.2 | RA | 0.4 ± 0.1 | - | - | ||
| CVN-WM | 100% | - | - | - | - | ||||||
| CVN-FL | 50% | 25% | 25% | - | - | ||||||
| CVN-HAZ | - | 16.7% | 16.7% | 16.6% | 50% | ||||||
| LHW | Structure size (μm) | PCG-W | 68.8 ± 7.1 | PAG | 36.1 ± 5.6 | PAG | - | PAG-W | 6.4 ± 2.5 | PAG-W | 6.4 ± 2.5 |
| AF | 1.5 ± 0.9 | Packet | 4.2 ± 2.8 | QPF | 4.2 ± 1.6 | QPF | 3.8 ± 1.4 | Packet | 11.2 ± 3.8 | ||
| GBF-W | 18.5 ± 10.1 | Block | 3.4 ± 1.6 | M/A | 1.4 ± 0.5 | M/A | 1.3 ± 0.4 | Block | 2.4 ± 0.5 | ||
| RA | 0.6 ± 0.2 | RA | 0.7 ± 0.1 | RA | 0.3 ± 0.1 | RA | 0.4 ± 0.2 | - | - | ||
| CVN-WM | 100% | - | - | - | - | ||||||
| CVN-FL | 50% | 16.7% | 16.7% | 16.6% | - | ||||||
| CVN-HAZ | - | 16.7% | 16.7% | 16.6% | 50% | ||||||
Table 3 Size of the microstructures formed in welded zone and BM of the studied steel, and the proportion of each sub region contained in the impact sample
| Welding method | Size and proportion | WM | CGHAZ | FGHAZ | ICHAZ | BM | |||||
|---|---|---|---|---|---|---|---|---|---|---|---|
| SAW | Structure size (μm) | PCG-W | 81.2 ± 11.4 | PAG | 42.7 ± 6.3 | PAG | - | PAG-W | 6.4 ± 2.5 | PAG-W | 6.4 ± 2.5 |
| AF | 2.1 ± 1.3 | Packet | 4.7 ± 3.2 | QPF | 4.6 ± 2.2 | QPF | 2.8 ± 1.5 | Packet | 11.2 ± 3.8 | ||
| GBF-W | 28.3 ± 13.5 | Block | 7.7 ± 5.4 | M/A | 1.8 ± 0.7 | M/A | 1.6 ± 0.6 | Block | 2.4 ± 0.5 | ||
| RA | 0.8 ± 0.3 | RA | 0.8 ± 0.2 | RA | 0.4 ± 0.2 | RA | 0.4 ± 0.1 | - | - | ||
| CVN-WM | 100% | - | - | - | - | ||||||
| CVN-FL | 50% | 25% | 25% | - | - | ||||||
| CVN-HAZ | - | 16.7% | 16.7% | 16.6% | 50% | ||||||
| LHW | Structure size (μm) | PCG-W | 68.8 ± 7.1 | PAG | 36.1 ± 5.6 | PAG | - | PAG-W | 6.4 ± 2.5 | PAG-W | 6.4 ± 2.5 |
| AF | 1.5 ± 0.9 | Packet | 4.2 ± 2.8 | QPF | 4.2 ± 1.6 | QPF | 3.8 ± 1.4 | Packet | 11.2 ± 3.8 | ||
| GBF-W | 18.5 ± 10.1 | Block | 3.4 ± 1.6 | M/A | 1.4 ± 0.5 | M/A | 1.3 ± 0.4 | Block | 2.4 ± 0.5 | ||
| RA | 0.6 ± 0.2 | RA | 0.7 ± 0.1 | RA | 0.3 ± 0.1 | RA | 0.4 ± 0.2 | - | - | ||
| CVN-WM | 100% | - | - | - | - | ||||||
| CVN-FL | 50% | 16.7% | 16.7% | 16.6% | - | ||||||
| CVN-HAZ | - | 16.7% | 16.7% | 16.6% | 50% | ||||||
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