Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (9): 1547-1558.DOI: 10.1007/s40195-022-01385-8
Special Issue: 腐蚀-1 2022; Mg合金 2022
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Xiu-Rong Zhu1, Jun Wang1(
), Wei-Ning Shi2, Xue-Bing Liu2, Xin-Fang Zhang2(
), Hai-Fei Zhou3
Received:2021-11-10
Revised:2021-11-24
Accepted:2021-11-29
Online:2022-09-10
Published:2022-02-15
Contact:
Jun Wang,Xin-Fang Zhang
About author:Xin-Fang Zhang, xfzhang@ustb.edu.cnXiu-Rong Zhu, Jun Wang, Wei-Ning Shi, Xue-Bing Liu, Xin-Fang Zhang, Hai-Fei Zhou. Manipulating Precipitation Through Thermomechanical Treatment to Control Corrosion Behavior of an Al-Cu-Mg Alloy[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(9): 1547-1558.
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| Sample ID | Solution treatment (495 °C) | Peak aging (190 °C) | Retrogression treatment (280 °C) | Cold rolling deformation | Natural aging (NA) |
|---|---|---|---|---|---|
| A | 1 h | - | - | - | 7 days |
| B | 1 h | - | - | 30% | 7 days |
| C | 1 h | - | - | 50% | 7 days |
| D | 1 h | - | - | 70% | 7 days |
| E | 1 h | 20 h | 20 min | - | 7 days |
| F | 1 h | 20 h | 20 min | 30% | 7 days |
| G | 1 h | 20 h | 20 min | 50% | 7 days |
| H | 1 h | 20 h | 20 min | 70% | 7 days |
Table 1 Detailed processing parameters of the studied Al-Cu-Mg alloys
| Sample ID | Solution treatment (495 °C) | Peak aging (190 °C) | Retrogression treatment (280 °C) | Cold rolling deformation | Natural aging (NA) |
|---|---|---|---|---|---|
| A | 1 h | - | - | - | 7 days |
| B | 1 h | - | - | 30% | 7 days |
| C | 1 h | - | - | 50% | 7 days |
| D | 1 h | - | - | 70% | 7 days |
| E | 1 h | 20 h | 20 min | - | 7 days |
| F | 1 h | 20 h | 20 min | 30% | 7 days |
| G | 1 h | 20 h | 20 min | 50% | 7 days |
| H | 1 h | 20 h | 20 min | 70% | 7 days |
Fig. 4 Precipitates and dislocation structures on grain boundaries of samples a A, b B, c C, d D, e line scanning analysis at yellow line position of sample B, f composition at yellow line position in e
Fig. 5 Secondary phases and dislocation structures within the grain interiors in the solution-treated series Al-Cu-Mg alloys. a sample A, b sample B (inset shows the SAED pattern of the T-phase), c sample C, d sample D (inset shows the SAED pattern of the matrix), e composition of the T-phase shown in a
Fig. 6 S-phase precipitates and dislocations on grain boundaries of retrogression-treated series Al-Cu-Mg alloy: a sample E, b sample F, c dislocations near the grain boundaries of sample F, d composition of the S-phase shown in a, e sample G, f sample H
Fig. 8 Dislocations and secondary phases in grain interiors of retrogression-treated series Al-Cu-Mg alloy: a sample E, b sample F, c S-phase in grain interiors of sample F (inset shows the SAED pattern of the S-phase), d composition of S-phase shown in (c), e sample G, f sample H
Fig. 9 Coherent relationship between S-phase and Al matrix in sample F: a morphology of S-phase, b composition of S-phase shown in a, c HRTEM of S-phase shown in a, d partially enlarged view of c, e FFT results of S-phase in c, f FFT results of Al matrix in c
Fig. 10 XRD test and analysis results of the alloys with retrogression treatment, 30-70% cold rolling deformation and natural aging: a XRD test results, b fitting result of sample F, c fitting result of sample G, d fitting result of sample H
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