Acta Metallurgica Sinica (English Letters) ›› 2021, Vol. 34 ›› Issue (12): 1695-1703.DOI: 10.1007/s40195-021-01232-2
Special Issue: 2021年钢铁专辑-1
Previous Articles Next Articles
Honglin Yan1,2, Zhiming Zhang1(
), Jianqiu Wang1, Bright O. Okonkwo1,2, En-Hou Han1
Received:2020-11-09
Revised:2021-01-18
Accepted:2021-01-26
Online:2021-12-10
Published:2021-12-10
Contact:
Zhiming Zhang
About author:Zhiming Zhang zmzhang@imr.ac.cnHonglin Yan, Zhiming Zhang, Jianqiu Wang, Bright O. Okonkwo, En-Hou Han. Effects of MeV Fe Ions Irradiation on the Microstructure and Property of Nuclear Grade 304 Stainless Steel: Characterized by Positron Annihilation Spectroscopy, Transmission Electron Microscope and Nanoindentation[J]. Acta Metallurgica Sinica (English Letters), 2021, 34(12): 1695-1703.
Add to citation manager EndNote|Ris|BibTeX
| C | Cr | Ni | N | Mn | Si | S | P | Fe |
|---|---|---|---|---|---|---|---|---|
| 0.053 | 18.45 | 8.30 | 0.057 | 1.59 | 0.47 | 0.004 | 0.022 | Bal. |
Table 1 Chemical composition of 304SS (wt%)
| C | Cr | Ni | N | Mn | Si | S | P | Fe |
|---|---|---|---|---|---|---|---|---|
| 0.053 | 18.45 | 8.30 | 0.057 | 1.59 | 0.47 | 0.004 | 0.022 | Bal. |
Fig. 2 Schematic diagram of S and W parameters in Doppler broadening of PAS. S represents the fractional area of the central portion of the peak, while W parameter is the fractional area of the extreme wings of the photo-peak
Fig. 7 Morphologies of the cross sections of the irradiated samples: a bright-field TEM image of 3.2 dpa sample, b morphology of irradiation-induced defects of 3.2 dpa sample, c bright-field TEM image of 16 dpa sample, d morphology of irradiation-induced defects of 16 dpa sample
Fig. 9 SEM micrographs of the all samples after indentation tests. Note that surface morphologies were different that grain boundaries were clear for unirradiated sample, while it became obscure for the irradiated samples
Fig. 10 Dependence of nanohardness of 304SS on the indentation depth of a unirradiated sample, b irradiated for 3.2 dpa, c irradiated for 16 dpa, d Hirr/Hunirr versus depth plot of all samples
| 304SS (dpa) | H0 (GPa) | h* (nm) | hcrit (nm) | ΔH0/H0 (irradiation hardening) |
|---|---|---|---|---|
| 0 dpa | 3.01 | 101.4 | 200 | - |
| 3.2 dpa | 4.67 | 49.3 | 200 | 55% |
| 16 dpa | 5.16 | 17.8 | 200 | 71% |
Table 2 Nix-Gao model plot results
| 304SS (dpa) | H0 (GPa) | h* (nm) | hcrit (nm) | ΔH0/H0 (irradiation hardening) |
|---|---|---|---|---|
| 0 dpa | 3.01 | 101.4 | 200 | - |
| 3.2 dpa | 4.67 | 49.3 | 200 | 55% |
| 16 dpa | 5.16 | 17.8 | 200 | 71% |
| 304SS (dpa) | H0 (GPa) | \(\Delta H_{v}\)(MPa) | \(\Delta \sigma_{y}\)(MPa) | \(\Delta \sigma_{y}^{\prime }\)(MPa) |
|---|---|---|---|---|
| 0 | 3.01 | 0 | 0 | 0 |
| 3.2 | 4.67 | 156.9 | 475.3 | 1367.5 |
| 16 | 5.16 | 203.2 | 615.6 | 975.6 |
Table 3 Comparison of hardness and yield strength of all samples
| 304SS (dpa) | H0 (GPa) | \(\Delta H_{v}\)(MPa) | \(\Delta \sigma_{y}\)(MPa) | \(\Delta \sigma_{y}^{\prime }\)(MPa) |
|---|---|---|---|---|
| 0 | 3.01 | 0 | 0 | 0 |
| 3.2 | 4.67 | 156.9 | 475.3 | 1367.5 |
| 16 | 5.16 | 203.2 | 615.6 | 975.6 |
| [1] | W.M. Tian, Y.J. Ai, S.M. Li, N. Du, C. Ye, Acta Metall. -Engl.Lett. 28, 430(2015) |
| [2] | S.J. Zinkle, G.S. Was, Acta Mater. 61, 735(2013) |
| [3] | W.C. Dong, D.B. Gao, S.P. Lu, Acta Metall. -Engl. Lett. 32, 618(2018) |
| [4] | M.N. Gussev, E. Cakmak, K.G. Field, J. Nucl. Mater. 504, 221(2018) |
| [5] | G.S. Was, S.M. Bruemmer, J. Nucl. Mater. 216, 326(1994) |
| [6] | A.B. Du, W. Feng, H.L. Ma, T. Liang, D.Q. Yuan, P. Fan, Q.L. Zhang, C. Huang, Acta Metall. -Engl. Lett. 30, 1049(2017) |
| [7] | S.J. Zinkle, Phys. Plasmas 12, 058101 (2005) |
| [8] | G.S. Was, J.T. Busby, Philos. Mag. 85, 443(2006) |
| [9] | P. Scott, J. Nucl. Mater. 211, 101(1994) |
| [10] | Z. Jiao, G.S. Was, J. Nucl. Mater. 382, 203(2008) |
| [11] | P.L. Andresen, M.M. Morra, J. Nucl. Mater. 383, 97(2008) |
| [12] | G.S. Was, Z. Jiao, E. Getto, K. Sun, A.M. Monterrosa, S.A. Maloy, O. Anderoglu, B.H. Sencer, M. Hackett, Scr. Mater. 88, 33(2014) |
| [13] | G.S. Was, J. Mater. Res. 30, 1158(2015) |
| [14] | R. Kasada, S. Konishi, K. Yabuuchi, S. Nogami, M. Ando, D. Hamaguchi, H. Tanigawa, Fusion Eng. Des. 89, 1637(2014) |
| [15] | J. Gupta, J. Hure, B. Tanguy, L. Laffont, M.C. Lafont, E. Andrieu, J. Nucl. Mater. 476, 82(2016) |
| [16] | G. S. Was, R. S. Averback. in Comprehensive Nuclear Materials (Elsevier Ltd, 2012), pp. 195. |
| [17] | Z.J. Jiao, G. Was, T. Miura, K. Fukuya, J. Nucl. Mater. 452, 328 (2014) |
| [18] | C.D. Hardie, S.G. Roberts, A.J. Bushby, J. Nucl. Mater. 462, 391 2015) |
| [19] | P. Hosemann, D. Kiener, Y.Q. Wang, S.A. Maloy, J. Nucl. Mater. 425, 136(2012) |
| [20] | S. Dannefaer, G.W. Dean, D.P. Kerr, B.G. Hogg, Phys. Rev. B 14, 2709 (1976) |
| [21] | J.F. Ziegler, M.D. Ziegler, J.P. Biersack, Nucl. Instrum. Methods Phys. Res. Sect. B 268, 1818 (2010) |
| [22] | R.E. Stoller, M.B. Toloczko, G.S. Was, A.G. Certain, S. Dwaraknath, F.A. Garner, Nucl. Instrum. Methods Phys. Res. Sect. B 310, 75 (2013) |
| [23] | S.J. Zinkle, L.L. Snead, Scr. Mater. 143, 154(2018) |
| [24] | H.P. Zhu, Z.G. Wang, X. Gao, M.H. Cui, B.S. Li, J.R. Sun, C.F. Yao, K.F. Wei, T.L. Shen, L.L. Pang, Y.B. Zhu, Y.F. Li, J. Wang, P. Song, P. Zhang, X.Z. Cao, Nucl. Instrum. Methods Phys. Res. Sect. B 344, 5 (2015) |
| [25] | C. Pokor, Y. Brechet, P. Dubuisson, J.P. Massoud, A. Barbu, J. Nucl. Mater. 326, 19(2004) |
| [26] | W.C. Oliver, G.M. Pharr, J. Mater. Res. 7, 1564(2011) |
| [27] | J. Algers, P. Sperr, W. Egger, G. Kögel, F.H.J. Maurer, Phys. Rev. B 67, 125404 (2003) |
| [28] | A.P. Mills, R.J. Wilson, Phys. Rev. A 26, 490 (1982) |
| [29] | J. Mákinen, A. Vehanen P. Hautojárvi H. Huomo J. Lahtinen R.M. Nieminen S. Valkealahti, Surf Sci. 175, 385(1986) |
| [30] | D.T. Britton, P.C. Riceevans, J.H. Evans, Phil. Mag. Lett. 57, 165(1988) |
| [31] | H. Zhu, Z.G. Wang, M.H. Cui, B.S. Li, X. Gao, J.R. Sun, C.F. Yao, K.F. Wei, T.L. Shen, L.L. Pang, Y.B. Zhu, Y.F. Li, J. Wang, E.Q. Xie, Appl. Surf. Sci. 326, 1(2015) |
| [32] | Q. Xu, K. Sato, X.Z. Cao, P. Zhang, B.Y. Wang, T. Yoshiie, H. Watanabe, N. Yoshida, Nucl. Instrum. Methods Phys. Res. Sect. B 315, 146 (2013) |
| [33] | X.B. Liu, R.S. Wang, J. Jiang, Y.C. Wu, C.H. Zhang, A. Ren, C.L. Xu, W.J. Qian, J. Nucl. Mater. 451, 249(2014) |
| [34] | P.J. Maziasz, J. Nucl. Mater. 205, 118(1993) |
| [35] | D.J. Edwards, E.P. Simonen, S.M. Bruemmer, J. Nucl. Mater. 317, 13(2003) |
| [36] | Z.C. Zheng, Y.X. Yu, W.P. Zhang, Z.Y. Shen, F.F. Luo, L.P. Guo, Y.Y. Ren, R. Tang, Acta Metall. -Engl. Lett. 30, 89(2016) |
| [37] | B.H. Sencer, G.M. Bond, M.L. Hamilton, F.A. Garner, S.A. Maloy, W.F. Sommer, J. Nucl. Mater. 296, 112(2001) |
| [38] | J. Malaplate, B. Michaut, A.R. Laborne, T. Jourdan, F. Dalle, J. Ribis, B. Radiguet, F. Sefta, B. Decamps, J. Nucl. Mater. 517, 201(2019) |
| [39] | E.H. Lee, Y. Lee, W.C. Oliver, L.K. Mansur, J. Mater. Res. 8, 377(2011) |
| [40] | K. Yabuuchi, Y. Kuribayashi, S. Nogami, R. Kasada, A. Hasegawa, J. Nucl. Mater. 446, 142(2014) |
| [41] | C.D. Hardie, S.G. Roberts, J. Nucl. Mater. 433, 174(2013) |
| [42] | W.D. Nix, H.J. Gao. J. Mech. Phys. Solids 46, 411 (1998) |
| [43] | R. Kasada, Y. Takayama, K. Yabuuchi, A. Kimura, Fusion Eng. Des. 86, 2658(2011) |
| [44] | A. Lupinacci, K. Chen, Y. Li, M. Kunz, Z. Jiao, G.S. Was, M.D. Abad, A.M. Minor, P. Hosemann, J. Nucl. Mater. 458, 70(2015) |
| [45] | J.T. Busby, M.C. Hash, G.S. Was, J. Nucl. Mater. 336, 267(2005) |
| [46] | C. Pokor, Y. Brechet, P. Dubuisson, J.P. Massoud, X. Averty, J. Nucl. Mater. 326, 30(2004) |
| [47] | A. K. Seeger, Report No. A/CONF. 15/P/998, 1959. |
| [48] | A.S. Rao, Nucl. Eng. Des. 269, 78(2014) |
| [49] | O. El-Atwani, J.S. Weaver, E. Esquivel, M. Efe, M.R. Chancey, Y.Q. Wang, S.A. Maloy, N. Mara, J. Nucl. Mater. 509, 276(2018) |
| [1] | Zheng-Hong Liu, Ying Han, Jia-Peng Sun, Ming-Kun Jiang, Ying Song, Guo-Qing Zu, Xu Ran. A Novel Cu-Modified 20Cr Lean Duplex Stainless Steel with Exceptional Combination of Mechanical Properties and Corrosion Resistance [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(8): 1361-1370. |
| [2] | Yuntian Lou, Shengyu He, Xudong Chen, Weiwei Chang, Hao Zhang, Jingzhi Yang, Hongchang Qian, Dawei Zhang. Effect of Ultrasonic Shot Peening on the Corrosion Resistance and Antibacterial Properties of 304 Cu-Bearing Stainless Steel [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(8): 1371-1384. |
| [3] | Li Zhao, Tian-Yu Cui, Wei-Wei Chang, Hong-Chang Qian, Yun-Tian Lou, Jing-Zhi Yang, Da-Wei Zhang. Effect of Mineralization Induced by Shewanella algae on Passive Film of Stainless Steel via FIB-SEM/TEM and EELS [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(6): 877-888. |
| [4] | Yifan Li, Shengyao Ma, Xinrui Zhang, Tong Xi, Chunguang Yang, Hanyu Zhao, Ke Yang. Copper Precipitation Behavior and Mechanical Properties of Cu-Bearing Ferritic Stainless Steel with Different Cr Addition [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(3): 383-395. |
| [5] | Ji-Peng Yang, Hai-Feng Zhang, Hong-Chao Ji, Nan Jia. Molecular Dynamics Simulations of Micromechanical Behaviours for AlCoCrFeNi2.1 High Entropy Alloy during Nanoindentation [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(2): 218-232. |
| [6] | Chenghao Liu, Wenchao Dong, Jian Sun, Shanping Lu. Effect of Precipitation Behavior and Deformation Twinning Evolution on the Mechanical Properties of 16Cr-25.5Ni-4.2Mo Superaustenitic Stainless Steel Weld Metals [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(2): 338-352. |
| [7] | Yiran Xiong, Ziyu Zhang, Xinqiang Wu, Jibo Tan, Xiang Wang. Dissolution Behaviors of Corrosion Products on 316LN Stainless Steel in Simulated Shutdown Acid-Reducing Water Chemistry [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(12): 2289-2299. |
| [8] | Yakui Chen, Shitong Wei, Dong Wu, Shanping Lu. Effects of Aging at 550 °C on α′-Martensitic Transformation of High Si-Bearing Metastable Austenitic Stainless Steel Weld Metal [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(9): 1467-1479. |
| [9] | Erika Lannunziata, Mohammad Hossein Mosallanejad, Manuela Galati, Gabriele Piscopo, Abdollah Saboori. Analyzing the Interplay of Sintering Conditions on Microstructure and Hardness in Indirect Additive Manufacturing of 17-4PH Stainless Steel [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(9): 1611-1620. |
| [10] | Hong-Wei Zhang, Li-Wei Lan, Zhe-Yu Yang, Chang-Chun Li, Wen-Xian Wang. Microstructure Evolution and Nanomechanical Behavior of Micro-Area in Molten Pool of Selective Laser Melting (CoCrNi)82Al9Ti9 High-Entropy Alloy [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(6): 1019-1033. |
| [11] | Pengwei Jiang, Gang Wang, Yaosha Wu, Zhigang Zheng, Zhaoguo Qiu, Tongchun Kuang, Jibo Huang, Dechang Zeng. Microstructure Evolution, Tribological and Corrosion Properties of Amorphous Alloy Strengthening Stainless Steel Fabricated by Selective Laser Melting in NaCl Solution [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(5): 825-839. |
| [12] | Dongqiqiong Wang, Qiang Wang, Xiaowu Li, Zhefeng Zhang. Improving Fatigue Properties of 316L Stainless Steel Welded Joints by Surface Spinning Strengthening [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(5): 840-854. |
| [13] | Yiqi Zhou, Decheng Kong, Ruixue Li, Xing He, Chaofang Dong. Corrosion of Duplex Stainless Steel Manufactured by Laser Powder Bed Fusion: A Critical Review [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(4): 587-606. |
| [14] | Andrea Kellenberger, Nicolae Vaszilcsin, Mircea Laurentiu Dan, Ion Mitelea, Alexandru Adrian Geana, Sigrid Lædre, Corneliu M. Craciunescu. Corrosion Investigation by Scanning Electrochemical Microscopy of AISI 446 and Ti-Coated AISI 446 Ferritic Stainless Steel as Potential Material for Bipolar Plate in PEMWE [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(4): 607-619. |
| [15] | Zhenghong Liu, Zhigang Wu, Ying Han, Xiaolei Song, Guoqing Zu, Weiwei Zhu, Xu Ran. Combination of High Yield Strength and Improved Ductility of 21Cr Lean Duplex Stainless Steel by Tailoring Cold Deformation and Low-Temperature Short-Term Aging [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(4): 695-702. |
| Viewed | ||||||
|
Full text |
|
|||||
|
Abstract |
|
|||||
WeChat
