Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (3): 354-368.DOI: 10.1007/s40195-021-01290-6
Special Issue: 2022年增材制造专辑
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Minbo Wang1, Ruidi Li1, Tiechui Yuan1(
), Haiou Yang2(
), Pengda Niu1, Chao Chen1
Received:2021-04-08
Revised:2021-05-29
Accepted:2021-06-14
Online:2021-08-31
Published:2021-08-31
Contact:
Tiechui Yuan,Haiou Yang
About author:Haiou Yang, yanghaiou@nwpu.edu.cnMinbo Wang, Ruidi Li, Tiechui Yuan, Haiou Yang, Pengda Niu, Chao Chen. Microstructure and Mechanical Properties of Selective Laser Melted Al-2.51Mn-2.71Mg-0.55Sc-0.29Cu-0.31Zn Alloy Designed by Supersaturated Solid Solution[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(3): 354-368.
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| Mn | Mg | Sc | Zr | Si | Cu | Zn | Al |
|---|---|---|---|---|---|---|---|
| 2.51 | 2.71 | 0.55 | 0.41 | 0.77 | 0.29 | 0.31 | Balance |
Table 1 Chemical composition of raw Al-Mn-Mg-Sc alloy powder (wt%)
| Mn | Mg | Sc | Zr | Si | Cu | Zn | Al |
|---|---|---|---|---|---|---|---|
| 2.51 | 2.71 | 0.55 | 0.41 | 0.77 | 0.29 | 0.31 | Balance |
Fig. 4 OM images of the SLM Al-Mn-Mg-Sc samples with different laser energy densities: a, a1 Q = 58.3 J/mm3; b, b1 Q = 62.5 J/mm3; c, c1 Q = 66.7 J/mm3; d, d1 Q = 75 J/mm3; building direction: a-d; scanning direction: a1-d1
Fig. 7 Tensile strength of the SLM and HT samples with various laser energy density: a calculated UTS, YS and ${\varepsilon }_{\mathrm{f}}$; b stress-strain curves during tensile test
Fig. 8 Inverse pole figure, kernel average misorientation of Al-Mn-Mg-Sc alloy (Q = 66.7 J/mm3): a, b IPF maps; c, d KAM maps; a, c building direction; b, d scanning direction
Fig. 9 Grain size distribution a, b and misorientation angle distribution c, d of SLM Al-Mn-Mg-Sc samples in building direction a, c and scanning direction (b, d)
Fig. 10 PFs showing the {100} crystallographic orientation of SLM Al-Mn-Mg-Sc samples in building direction a and scanning direction b; c standard (001) stereographic projectionFull size image
Fig. 13 Morphologies of the different crystal structure in building direction: a, d FEG; b CD; c CEG; e contrast between FEG and CD; f contrast between FEG and CEG
Fig. 15 TEM images of sample processed by SLM: a bright-field TEM image of the building direction; b SAED pattern from a, showing the diffraction patterns of phases
Fig. 16 BFTEM and HRTEM images of FEG zone in building direction: a high density dislocations in BFTEM; b, c detailed dislocation pile up group in HRTEM; d vacancies and thickness fringes in BFTEM; e, f detailed thickness fringes in HRTEM
Fig. 17 a HRTEM images of CEG zone showing the crystalline structure of precipitations in CEG zone; b matrix α-Al with FCC structure; c, f the transformation of α-Al matrix to Al3(Sc, Zr) particle; d, e Al3(Sc, Zr) particle with L12 structure
| [1] |
J. Zhang, B. Song, Q. Wei, D. Bourell, Y. Shi, J. Mater. Sci. Technol. 35, 270 (2019)
DOI URL |
| [2] |
E.O. Olakanmi, R.F. Cochrane, K.W. Dalgarno, Prog. Mater. Sci. 74, 401 (2015)
DOI URL |
| [3] |
W. Xu, M. Brandt, S. Sun, J. Elambasseril, Q. Liu, K. Latham, K. Xia, M. Qian, Acta Mater. 85, 74 (2015)
DOI URL |
| [4] |
R.R. Dehoff, S.S. Babu, Acta Mater. 58, 4305 (2010)
DOI URL |
| [5] |
M. Vlach, I. Stulikova, B. Smola, T. Kekule, H. Kudrnova, S. Danis, R. Gemma, V. Ocenasek, J. Malek, D. Tanprayoon, V. Neubert, Mater. Charact. 86, 59 (2013)
DOI URL |
| [6] | B. Forbord, H. Hallem, N. Ryum, K. Marthinsen, Mater. Sci. Eng. A 387-389, 936(2004) |
| [7] | F. Jiang, H. Zhang, X. Ji, X. Meng, L. Li, Mater. Sci. Eng. A 595, 10 (2014) |
| [8] |
K. Liu, A.M. Nabawy, X.G. Chen, Trans. Nonferrous Met. Soc. China 27, 771 (2017)
DOI URL |
| [9] |
K. Liu, X.G. Chen, Mater. Sci. Eng. A 697, 141 (2017)
DOI URL |
| [10] |
K. Liu, H. Ma, X.G. Chen, J. Alloys Compd. 694, 354 (2017)
DOI URL |
| [11] |
K.L. Kendig, D.B. Miracle, Acta Mater. 50, 4165 (2002)
DOI URL |
| [12] |
O.N. Senkov, M.R. Shagiev, S.V. Senkova, D.B. Miracle, Acta Mater. 56, 3723 (2008)
DOI URL |
| [13] |
M.E. Krug, Z. Mao, D.N. Seidman, D.C. Dunand, Acta Mater. 79, 382 (2014)
DOI URL |
| [14] |
M. Vlach, I. Stulíková, B. Smola, N. Žaludová, Mater. Charact. 61, 1400 (2010)
DOI URL |
| [15] | M. Vlach, I. Stulikova, B. Smola, J. Piesova, H. Cisarova, S. Danis, J. Plasek, R. Gemma, D. Tanprayoon, V. Neubert, Mater. Sci. Eng. A 548, 27 (2012) |
| [16] | A.B. Spierings, K. Dawson, K. Kern, F. Palm, K. Wegener, Mater. Sci. Eng. A 701, 264 (2017) |
| [17] | T. Yu, J. Liu, Y. He, J. Tian, M. Chen, Y. Wang, Wear 476, 203581 (2021). |
| [18] |
A.B. Spierings, K. Dawson, P.J. Uggowitzer, K. Wegener, Mater. Des. 140, 134 (2018)
DOI URL |
| [19] |
R. Li, M. Wang, T. Yuan, B. Song, C. Chen, K. Zhou, P. Cao, Powder Technol. 319, 117 (2017)
DOI URL |
| [20] | M. Wang, R. Li, T. Yuan, C. Chen, L. Zhou, H. Chen, M. Zhang, S. Xie, Mater. Sci. Eng. A 756, 354 (2019) |
| [21] |
Q. Jia, P. Rometsch, P. Kürnsteiner, Q. Chao, A. Huang, M. Weyland, L. Bourgeois, X. Wu, Acta Mater. 171, 108 (2019)
DOI URL |
| [22] | H. Asgari, C. Baxter, K. Hosseinkhani, M. Mohammadi, Mater. Sci. Eng. A 707, 148 (2017) |
| [23] | W. Li, S. Li, J. Liu, A. Zhang, Y. Zhou, Q. Wei, C. Yan, Y. Shi, Mater. Sci. Eng. A 663, 116 (2016) |
| [24] |
A.B. Spierings, K. Dawson, T. Heeling, P.J. Uggowitzer, R. Schäublin, F. Palm, K. Wegener, Mater. Des. 115, 52 (2017)
DOI URL |
| [25] |
R. Li, M. Wang, Z. Li, P. Cao, T. Yuan, H. Zhu, Acta Mater. 193, 83 (2020)
DOI URL |
| [26] |
Y.K. Kim, J. Choe, K.A. Lee, J. Alloys Compd. 805, 680 (2019)
DOI URL |
| [27] |
Z. Zribi, H.H. Ktari, F. Herbst, V. Optasanu, N. Njah, Mater. Charact. 153, 190 (2019)
DOI URL |
| [28] | Y. Shi, K. Yang, S.K. Kairy, F. Palm, X. Wu, P.A. Rometsch, Mater. Sci. Eng. A 732, 41 (2018) |
| [29] |
W. Li, Y. Yang, J. Liu, Y. Zhou, M. Li, S. Wen, Q. Wei, C. Yan, Y. Shi, Acta Mater. 136, 90 (2017)
DOI URL |
| [30] | J. Bi, Z. Lei, Y. Chen, X. Chen, Z. Tian, J. Liang, X. Zhang, X. Qin, Mater. Sci. Eng. A 768, 138478 (2019) |
| [31] | X. Yang, D. Wang, Z. Wu, J. Yi, S. Ni, Y. Du, M. Song, Mater. Sci. Eng. A 658, 16 (2016) |
| [32] |
J.H. Zheng, Y. Dong, K. Zheng, H. Dong, J. Lin, J. Jiang, T.A. Dean, J. Alloys Compd. 810, 151934 (2019)
DOI URL |
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