Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (12): 2013-2030.DOI: 10.1007/s40195-023-01608-6
Special Issue: 高温合金 2023
Previous Articles Next Articles
Hongyang Cui1,2, Yi Tan1,2, Rusheng Bai1,2, Lidan Ning1,2, Chuanyong Cui3, Xiaogang You4, Pengting Li1,2(
)
Received:2023-04-18
Revised:2023-08-22
Accepted:2023-08-23
Online:2023-12-10
Published:2023-10-30
Contact:
Pengting Li
Hongyang Cui, Yi Tan, Rusheng Bai, Lidan Ning, Chuanyong Cui, Xiaogang You, Pengting Li. Recrystallization Behavior of the New Ni-Co-Based Superalloy with Fusion Structure Produced by Electron Beam Smelting Layered Solidification Technology[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(12): 2013-2030.
Add to citation manager EndNote|Ris|BibTeX
| Co | Cr | W | Mo | Al + Ti | C + Zr + B | Ni |
|---|---|---|---|---|---|---|
| 20-26 | 13-15 | 1.1-1.3 | 2.4-2.8 | 7.72-8.40 | 0.04-0.11 | Bal. |
Table 1 Main composition of Ni-Co-based superalloy (wt%)
| Co | Cr | W | Mo | Al + Ti | C + Zr + B | Ni |
|---|---|---|---|---|---|---|
| 20-26 | 13-15 | 1.1-1.3 | 2.4-2.8 | 7.72-8.40 | 0.04-0.11 | Bal. |
Fig. 1 Microstructures of the new Ni-Co-based superalloy: a-a3 cast microstructures of EBSL-Ni-Co-based superalloy; b-b3 homogenized state microstructures of EBSL-Ni-Co-based superalloy; c-c3 homogenized state microstructures of DM-Ni-Co-based superalloy, d DSC curves of the EBSL-Ni-Co superalloy, d1 microstructure of the alloy solution treatment at 1120 °C for 10 min, d2 microstructure of the alloy solution treatment at 1160 °C for 10 min
Fig. 2 a Sampling requirements diagram; b schematic diagram of hot compression process schematic diagram; c the directions of sampling and characterization for EBSD and TEM tests
Fig. 3 Microstructures of the alloy after heat treatment at 1150 °C for 4 h: a EBSL-Ni-Co superalloy, b DM-Ni-Co superalloy, c grain size distribution map, d misorientation angle distribution map
Fig. 4 Corrected true stress-strain curves of the new Ni-Co superalloy under the hot deformed: a 1120 °C of EBSL-Ni-Co superalloy, b 1160 °C of EBSL-Ni-Co superalloy, c various microstructure, d schematic representations of the flow stress curve
Fig. 5 Microstructural characteristics of the new Ni-Co-based superalloy deformed at γ′ super-solvus temperature (1160 °C) to a strain rate of 0.01 s−1 with different strains: a-d DM-Ni-Co superalloy, e-h EBSL-Ni-Co superalloy
Fig. 6 Microstructural characteristics of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperatures to a strain of 0.7 with different strain rates: a-d γ′ sub -solvus temperatures (1120 °C), e-h γ′ super-solvus temperatures (1160 °C)
Fig. 7 a DRX grain volume fraction of different microstructures, b evolution of dislocation density inside a recrystallized grain during the DRX process, c the kernel average misorientation map for different deformation strains
Fig. 8 Distributions of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperature to a strain of 0.7 with different strain rates: a volume fraction of DRX grain, b volume fraction of LAGBs, MAGBs and HAGBs
Fig. 9 a DRX grain size distributions of the EBSL-Ni-Co superalloy deformed at γ′ sub-/super-solvus temperature to a strain of 0.7 with different strain rates, b schematic diagram of the interaction between a moving grain boundary and the dispersed γ′ phase, c, d microstructures at a strain rate of 0.01 s−1, e, f microstructures at a strain rate of 0.001 s−1
Fig. 10 Schematic diagram of the microstructure evolution deformed though DDRX: a IPF of regions G1 and the line graph, b misorientation angle along the arrow, c schematic diagram of microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphologies of the EBSL-Ni-Co superalloy
Fig. 11 Schematic diagram of the microstructure evolution deformed though CDRX: a IPF of regions G2, b the line graph and misorientation angle along the arrow, c microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphology of the EBSL-Ni-Co superalloy
Fig. 12 Schematic diagram of the microstructure evolution for the formation of TDRX: a, b IPF with strain 0.3, c microstructure deformed under EBSL-Ni-Co superalloy, d, e TEM morphology of the EBSL- Ni-Co superalloy
Fig. 13 Schematic diagram of the microstructure evolution deformed though PSN: a, b TEM morphologies of the EBSL-Ni-Co superalloy, c microstructure deformed under EBSL-Ni-Co-based superalloy
Fig. 14 Schematic illustration of grain refinement evolution and corresponding mechanisms during hot compression deformation: a γ′ sub-solvus temperature (1120 °C), b γ′ super-solvus temperature (1160 °C)
| 1. |
C.Y. Cui, Y.F. Gu, H. Harada, D.H. Ping, A. Sato, Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 37, 3183 (2006)
DOI URL |
| 2. | E.X. Pu, W.J. Zheng, Z.G. Song, H. Feng, H. Dong, Acta Metall. Sin. -Engl Lett. 30, 1119 (2017) |
| 3. |
H. Cui, Y. Tan, R. Bai, Y. Li, X. Zhuang, Z. Chen, X. You, P. Li, C. Cui, Mater. Charact. 184, 111668 (2022)
DOI URL |
| 4. |
H. Cui, Y. Tan, R. Bai, L. Ning, X. You, C. Cui, P. Li, J. Alloys Compd. 934, 167880 (2023)
DOI URL |
| 5. |
X. You, Y. Tan, M. Takeyama, P. Li, Y. Li, H. Zhang, H. Cui, C. Cui, Y. Wang, J. Li, Z. Zhang, G. Dong, W. Xiao, J. Mater. Sci. Technol. 143, 216 (2023)
DOI URL |
| 6. |
F. Liu, J. Chen, J. Dong, M. Zhang, Z. Yao, Mater. Sci. Eng. A 651, 102 (2016)
DOI URL |
| 7. | Y.T. Wang, J.B. Li, Y.C. Xin, X.H. Chen, M. Rashad, B. Liu, Y. Liu, Acta Metall. Sin. -Engl. Lett. 32, 932 (2019) |
| 8. |
G. Zhao, X. Zang, Y. Jing, N. Lü, J. Wu, Mater. Sci. Eng. A 815, 141293 (2021)
DOI URL |
| 9. |
M. Higashi, N. Kanno, Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 52, 181 (2021)
DOI |
| 10. |
Z. Zhou, R. Zhang, C. Cui, Y. Zhou, X. Sun, Mater. Sci. Eng. A 833, 142370 (2022)
DOI URL |
| 11. |
L. Zhao, Y. Tan, S. Shi, X. You, P. Li, C. Cui, J. Alloys Compd. 833, 155019 (2020)
DOI URL |
| 12. |
S. Dourandish, M. Jahazi, G.R. Ebrahimi, L. Ebacher, J. Mater. Res. Technol. 13, 260 (2021)
DOI URL |
| 13. | L. Zhang, W. Wang, M. Babar Shahzad, Y.Y. Shan, K. Yang, Acta Metall. Sin. -Engl. Lett. 32, 1161 (2019) |
| 14. | Y. Zhu, Y. Cao, R. Luo, C. Liu, H. Di, G. Shu, G. Huang, Q. Liu, Acta Metall. Sin. -Engl. Lett. 34, 1296 (2021) |
| 15. | Y.P. Li, R.B. Song, E.D. Wen, F.Q. Yang, Acta Metall. Sin. -Engl. Lett. 29, 441 (2016) |
| 16. | W.H. Qi, B.Y. Huang, M.P. Wang, Z. Li, Z.M. Yu, Phys. Lett. Sect. A Gen. At. Solid State Phys. 370, 494 (2007) |
| 17. |
B. Aashranth, M. Arvinth Davinci, D. Samantaray, U. Borah, S.K. Albert, Mater. Des. 116, 495 (2017)
DOI URL |
| 18. |
D.G. Cram, H.S. Zurob, Y.J.M. Brechet, C.R. Hutchinson, Acta Mater. 57, 5218 (2009)
DOI URL |
| 19. |
J. Hidalgo, M.J. Santofimia, Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 47, 5288 (2016)
DOI URL |
| 20. |
O. Beltran, K. Huang, R.E. Logé, Comput. Mater. Sci. 102, 293 (2015)
DOI URL |
| 21. | Y. Wu, Q. Hu, Z. Ding, J. Li, Acta Metall. Sin. -Engl. Lett. 36, 803 (2023) |
| 22. | C. Liu, J. Zhang, Y. Yang, X. Xia, T. He, J. Ding, Y. Tang, Z. Zhang, X. Chen, Y. Liu, Acta Metall. Sin. -Engl. Lett. 35, 1383 (2022) |
| 23. | J. Humphreys, G.S. Rohrer, A. Rollett, The Structure and Energy of Grain Boundaries, (Elsevier, Amsterdam 2017) |
| 24. | S. Huang, L. Wang, X. Lian, B. Zhang, G. Zhao, Acta Metall. Sin. -Engl. Lett. 27, 198 (2014) |
| 25. | J. Xun, G. Lin, H. Liu, S. Zhao, J. Chen, X. Dai, R. Zhang, Acta Metall. Sin. -Engl. Lett. 33, 215 (2020) |
| 26. |
A. Harte, M. Atkinson, A. Smith, C. Drouven, S. Zaefferer, J. Quinta da Fonseca, M. Preuss, Acta Mater. 194, 257 (2020)
DOI URL |
| 27. | F.J. Humphreys, M. Hatherly, Recrystallization and Related Annealing Phenomena, (Elsevier, Amsterdam 2012). |
| 28. | T.R. Afanasyev, Recrystallization in Metals and Alloys (1981). |
| 29. |
X. Tang, B. Wang, H. Ji, X. Fu, W. Xiao, Mater. Sci. Eng. A 675, 192 (2016)
DOI URL |
| 30. |
P. Liu, R. Zhang, Y. Yuan, C. Cui, F. Liang, X. Liu, Y. Gu, Y. Zhou, X. Sun, J. Mater. Sci. Technol. 77, 66 (2021)
DOI URL |
| 31. | M. Soucail, M. Marty, H. Octor, Superalloys (1996). |
| 32. | J.W. Martin, Encyclopedia of Materials: Science and Technology(Elsevier, Amsterdam, 2001), p.3634 |
| 33. | D. Zöllner, Ref. Modul. Mater. Sci. Mater. Eng. 30, 025010 (2016) |
| 34. |
V. Yadav, N. Moelans, Y. Zhang, D. Juul Jensen, Acta Mater. 221, 117377 (2021)
DOI URL |
| 35. | T. Sakai, Y. Nagao, M. Ohashi, J.J. Jonas, Mater. Sci. Technol. (United Kingdom) 2, 659 (1986) |
| 36. | T. Sakai, M. Ohashi, Mater. Sci. Technol. (United Kingdom) 6, 1251 (1990) |
| 37. | J. Humphreys, G.S. Rohrer, A. Rollett, Mobility and Migration of Boundaries, (Elsevier, Amsterdam 2017) |
| 38. |
B. Xie, H. Yu, T. Sheng, Y. Xiong, Y. Ning, M.W. Fu, J. Alloys Compd. 803, 16 (2019)
DOI URL |
| 39. | S. Wang, L. Wang, Y. Liu, G. Xu, B. Zhang, G. Zhao, Acta Metall. Sin. -Engl. Lett. 24, 295 (2011) |
| 40. | H.H. Lu, Y. Li, L. Lu, W.G. Zhang, W. Liang, Acta Metall. Sin. Engl. Lett. 35, 1983 (2022) |
| 41. |
V. Randle, Acta Mater. 52, 4067 (2004)
DOI URL |
| 42. |
H. Zhang, K. Zhang, H. Zhou, Z. Lu, C. Zhao, X. Yang, Mater. Des. 80, 51 (2015)
DOI URL |
| 43. |
L. Sun, Z. Xu, L. Peng, X. Lai, Scr. Mater. 219, 114877 (2022)
DOI URL |
| 44. | J. Humphreys, G.S. Rohrer, A. Rollett, Recrystallization and Related Annealing Phenomena(Elsevier, Amsterdam, 2017), p.305 |
| [1] | Biao Zhang, Yuntian Du, Huishuang Jia, Yuanyi Zhou, Liguang Wang, Minghe Zhang, Yunli Feng, Weimin Gao, Ning Xu. Hot Deformation Behavior of CoNiV Medium-Entropy Alloy: Constitutive Model, Convolutional Neural Network, Hot Processing Map, and Microstructure Evolution [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(8): 1275-1292. |
| [2] | Hongyang Zhang, Huihui Nie, Zhijian Li, Hongsheng Chen, Wei Liang, Liuwei Zheng. Evolution of Microstructure and Mechanical Properties of AZ31 Sheets with Different Initial Microstructures During the Corrugated Wide Limit Alignment Process [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(6): 1012-1028. |
| [3] | Tianyi Zeng, Zirui Luo, Hao Chen, Wei Wang, Ke Yang. Flow Behavior and Dynamic Recrystallization Mechanism of CSS-42L Bearing Steel During Hot Compression Deformation [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(3): 465-480. |
| [4] | Xiangru Guo, Jian Zhang, Tieqiang Kong, Junjie Shen, Qingjian Liu, Chaoyang Sun, Peipei Li. Unraveling the Discontinuous Dynamic Recrystallization of the TC17 Titanium Alloy during Hot Deformation by Crystal Plasticity Modeling [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(12): 2243-2264. |
| [5] | Rashad A. Al-Hammadi, Rui Zhang, Chuanyong Cui, Xipeng Tao, Yizhou Zhou. Deformation Mechanism and Fracture Behavior of a Coarse-Grain Ni-Co-Based Superalloy During Superplasticity [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(11): 2024-2034. |
| [6] | Fang-Fang Cao, Cui-Ju Wang, Kai-Bo Nie, Quan-Xin Shi, Yi-Jia Li, Kun-Kun Deng. Mechanical Properties and Work Hardening Behavior of Tip/Mg-Gd-Y-Zn Composites [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1777-1793. |
| [7] | Long Liu, Zijian Zhou, Jie Yu, Xinguang Wang, Chuanyong Cui, Rui Zhang, Yizhou Zhou, Xiaofeng Sun. Hot Deformation Behavior and Workability of a New Ni-W-Cr Superalloy for Molten Salt Reactors [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(8): 1453-1466. |
| [8] | Ping Li, Shuangwu Xia, Junfu Dong, Liangwei Dai, Zhicheng Luo, Kemin Xue. Effect of Bimodal Quasicrystal Phase on the Dynamic Recrystallization of Mg-Zn-Gd Alloy during High-Pressure Torsion [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(7): 1128-1134. |
| [9] | Rashad A. Al-Hammadi, Rui Zhang, Chuanyong Cui, Zijian Zhou, Yizhou Zhou. Revealing the Void Formation Mechanism during Superplastic Deformation of a Fine-Grained Ni-Co-Base Superalloy [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(5): 915-920. |
| [10] | Hengrui Hu, Jiayu Qin, Yunpeng Zhu, Jinhui Wang, Xiaoqiang Li, Peipeng Jin. Hot Deformation Behavior and Microstructures Evolution of GNP-Reinforced Fine-Grained Mg Composites [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(3): 407-424. |
| [11] | Yong-Chao Gai, Rui Zhang, Chuan-Yong Cui, Zi-Jian Zhou, Yi Tan, Yi-Zhou Zhou, Xiao-Feng Sun. Hot Compression Behavior and Tensile Property of a Novel Ni-Co-Based Superalloy Prepared by Electron Beam Smelting Layered Solidification Technology [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(2): 283-292. |
| [12] | Ke Qiao, Kuaishe Wang, Jia Wang, Zhengyang Hao, Kairui Xue, Jun Cai, Fengming Qiang, Wen Wang. Microstructure Evolution and Recrystallized Behavior of Friction Stir Welding Twin-Induced Plasticity Steel [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(11): 1947-1960. |
| [13] | Yanyang Wu, Qiaodan Hu, Zongye Ding, Jianguo Li. Effect of Grain Size and Compression Direction on the Hot Deformation Characteristics of High-Cr Ultra-Super-Critical Rotor Steel with Columnar Grains [J]. Acta Metallurgica Sinica (English Letters), 2023, 36(5): 803-813. |
| [14] | Bo Che, Liwei Lu, Longfei Liu, Yan Yang, Wei Kang, Jun Luo, Zhiqiang Wu, Yongfeng Qiu. Hot Compression Mechanical Behavior of Solution Heat-Treated and Pre-aged Mg-Zn-Gd-Er Alloys [J]. Acta Metallurgica Sinica (English Letters), 2023, 36(3): 469-485. |
| [15] | H. Zhang, H. L. Hao, G. Y. Fu, B. S. Liu, R. G. Li, R. Z. Wu, H. C. Pan. Microstructure and Mechanical Property of Hot-Rolled Mg-2Ag Alloy Prepared with Multi-pass Rolling [J]. Acta Metallurgica Sinica (English Letters), 2023, 36(2): 335-342. |
| Viewed | ||||||
|
Full text |
|
|||||
|
Abstract |
|
|||||
WeChat
