Acta Metallurgica Sinica (English Letters) ›› 2023, Vol. 36 ›› Issue (1): 1-20.DOI: 10.1007/s40195-022-01445-z
Special Issue: 2023年增材制造
Hua-Zhen Jiang1, Qi-Sheng Chen1,2,*(
), Zheng-Yang Li1,2,*(
), Xin-Ye Chen3, Hui-Lei Sun1, Shao-Ke Yao1,2, Jia-Huiyu Fang1,2, Qi-Yun Hu1,2
Received:2022-05-08
Revised:2022-06-07
Accepted:2022-06-21
Online:2023-01-10
Published:2022-08-16
Contact:
* Qi‑Sheng Chen, qschen@imech.ac.cn; Zheng‑Yang Li,zyli@imech.ac.cn
Hua-Zhen Jiang, Qi-Sheng Chen, Zheng-Yang Li, Xin-Ye Chen, Hui-Lei Sun, Shao-Ke Yao, Jia-Huiyu Fang, Qi-Yun Hu. Microstructure and Size-Dependent Mechanical Properties of Additively Manufactured 316L Stainless Steels Produced by Laser Metal Deposition[J]. Acta Metallurgica Sinica (English Letters), 2023, 36(1): 1-20.
Add to citation manager EndNote|Ris|BibTeX
Fig. 1 Experimental details in the study: a morphology of the as-used 316L SS powder, b a sketch of laser inside powder feeding nozzle, and c real photograph of the LMD system
| Fe | Cr | Ni | Mo | Mn | Si | C | P | S |
|---|---|---|---|---|---|---|---|---|
| Bal. | 19.30 ± 0.5 | 11.15 ± 0.65 | 1.70 ± 0.2 | 0.60 ± 0.3 | 1.40 ± 0.1 | ≤ 0.03 | ≤ 0.04 | ≤ 0.01 |
Table 1 Chemical composition of as-used 316L SS powders (wt%)
| Fe | Cr | Ni | Mo | Mn | Si | C | P | S |
|---|---|---|---|---|---|---|---|---|
| Bal. | 19.30 ± 0.5 | 11.15 ± 0.65 | 1.70 ± 0.2 | 0.60 ± 0.3 | 1.40 ± 0.1 | ≤ 0.03 | ≤ 0.04 | ≤ 0.01 |
| Laser power (W) | Beam diameter (mm) | Scanning speed (mm/s) | Powder feeding rate (g/min) | Hatch spacing (mm) | Layer thickness (mm) |
|---|---|---|---|---|---|
| 1100 | 2.0 | 6.0 | 10.3 | 1.0 | 0.2 |
Table 2 Optimal process parameters used in this work
| Laser power (W) | Beam diameter (mm) | Scanning speed (mm/s) | Powder feeding rate (g/min) | Hatch spacing (mm) | Layer thickness (mm) |
|---|---|---|---|---|---|
| 1100 | 2.0 | 6.0 | 10.3 | 1.0 | 0.2 |
Fig. 3 a Defects detection using OM method, b the corresponding distribution of defect size in terms of the major axis length in a, c OM image showing the columnar dendrites (e.g., region B) and cells (e.g., region A) in the material, the yellow and blue arrows indicate dendrites and cells, respectively, d SEM image revealing the solidification microstructure, e a magnified view showing the columnar dendrite and cell structures
Fig. 4 Microstructure of LMD-produced 316L SS sample observed by EBSD: a IQ map, b IPF image, c PF image, d band contrast map, e KAM map, f phase mapping, g misorientation angle distribution, and h grain size distribution
Fig. 5 A summary of mechanical properties versus specimen size for LMD-produced 316L SS samples: a yield strength, b ultimate tensile strength, c elongation to failure, and d slimness ratio dependence of elongation to failure with different specimen sizes
Fig. 6 Represented fracture surface of sample ‘S0.5-1’ (εf?=?12.9%). a Macroscopic fracture morphology, b, c are enlarged images showing the pore defects, d a high magnified image revealing the dimple fracture and oxide particles
Fig. 7 Represented fracture surface of sample ‘S1-1’ (εf?=?14.2%). a Macroscopic fracture morphology, b, c are enlarged images showing the pores and lack of fusion defects, d a high magnified image revealing the dimple fracture and oxide particles
Fig. 8 Represented fracture surface of sample ‘S2-2’ (εf?=?11.7%). a Macroscopic fracture morphology, b SEM image revealing the lack of fusion defects, c an enlarged image showing the pores, d a high magnified image revealing the dimple fracture and oxide particles
Fig. 9 Represented fracture surface of sample ‘w4.5-4’ (εf?=?12.2%). a Macroscopic fracture morphology, b, c enlarged images showing the dimple fracture and oxide particles
Fig. 10 Represented fracture surface of sample ‘w10-4’ (εf?=?15.7%). a Macroscopic fracture morphology, b SEM image revealing the pore defect, c a high magnified image revealing the dimple fracture and oxide particles
Fig. 11 Represented fracture surface of sample ‘w10-1’ (εf?=?35%). a Macroscopic fracture morphology, b, c are enlarged images showing the pores and lack of fusion defects, d a high magnified image revealing the dimple fracture and oxide particles
Fig. 12 Defect size distribution measured on the observed fracture surfaces. The corresponding area fraction of defect region is also presented. a Sample ‘S1-1’, b Sample ‘S2-2’, c Sample ‘S0.5-1’, d Sample ‘w10-1’, e Sample ‘w10-4’, f Sample ‘w4.5-4’
Fig. 13 OM and SEM images showing a representative side view of LMD-produced specimen after tensile testing: a OM image showing the crack propagates to the edge of fractured sample surface, b OM image showing the crack initiates from the pore, c SEM image showing an intergranular fracture mode
| Spectrum location | Element | |||||
|---|---|---|---|---|---|---|
| Si | Cr | Mn | Fe | Ni | Mo | |
| Oxide particles | 10.80 ± 1.61 | 27.11 ± 4.39 | 5.59 ± 2.93 | 45.25 ± 4.68 | 7.50 ± 1.00 | 2.36 ± 1.66 |
| 316L base material | 0.58 ± 0.37 | 20.68 ± 1.82 | 0.60 ± 0.32 | 64.53 ± 2.87 | 10.78 ± 2.19 | 2.48 ± 1.35 |
Table 3 EDS analysis results of oxide particles and LMD-produced 316L base from different sample fracture surfaces (wt%)
| Spectrum location | Element | |||||
|---|---|---|---|---|---|---|
| Si | Cr | Mn | Fe | Ni | Mo | |
| Oxide particles | 10.80 ± 1.61 | 27.11 ± 4.39 | 5.59 ± 2.93 | 45.25 ± 4.68 | 7.50 ± 1.00 | 2.36 ± 1.66 |
| 316L base material | 0.58 ± 0.37 | 20.68 ± 1.82 | 0.60 ± 0.32 | 64.53 ± 2.87 | 10.78 ± 2.19 | 2.48 ± 1.35 |
Fig. 14 A summary of yield strength versus elongation to failure for LMD-produced 316L SS from our work and previous studies [5,79,14,16,17,18,19]. The reported values are collected from different references where the LMD-produced samples are produced by different processing parameters and are tensile tested by various sample sizes and shapes
Fig. 15 Microstructures of deformed sample: a IQ map, b band contrast map, c IPF image, d KAM map, e grain size distribution, f misorientation angle distribution, g phase mapping
| [1] | D. Svetlizky, M. Das, B. Zheng, A.L. Vyatskikh, S. Bose, A. Bandyopadhyay, J.M. Schoenung, E.J. Lavernia, N. Eliaz, Mater. Today 49, 271 (2021) |
| [2] |
H.Z. Jiang, Z.Y. Li, T. Feng, P.Y. Wu, Q.S. Chen, Y.L. Fen, S.W. Li, H. Gao, H.J. Xu, Opt. Laser. Technol. 119, 105592 (2019)
DOI URL |
| [3] | H.Z. Jiang, Z.Y. Li, T. Feng, P.Y. Wu, Q.S. Chen, Y.L. Feng, L.F. Chen, J.Y. Hou, H. Xu, Acta Metall. Sin. 34, 495 (2020). (Engl. Lett.) |
| [4] |
Y. Zhong, L.F. Liu, S. Wikman, D.Q. Cui, Z.J. Shen, J. Nucl. Mater. 470, 170 (2016)
DOI URL |
| [5] | M. Ziętala, T. Durejko, M. Polański, I. Kunce, T. Płociński, W. Zieliński, M. Łazińska, W. Stępniowski, T. Czujko, K.J. Kurzydłowski, Z. Bojar, Mater. Sci. Eng. A 677, 1 (2016) |
| [6] | P. Kürnsteiner, M.B. Wilms, A. Weisheit, B. Gault, E.A. Jägle, D. Raabe,Nature 582, 515 (2020) |
| [7] | N. Li, Z. Li, Y. Wei,Nanomaterials 11, 2859 (2021) |
| [8] |
Y.M. Wang, T. Voisin, J.T. McKeown, J. Ye, N.P. Calta, Z. Li, Z. Zeng, Y. Zhang, W. Chen, T.T. Roehling, R.T. Ott, M.K. Santala, P.J. Depond, M.J. Matthews, A.V. Hamza, T. Zhu, Nat. Mater. 17, 63 (2018)
DOI URL |
| [9] | M. Ma, Z. Wang, X. Zeng, Mater. Sci. Eng. A 685, 265 (2017) |
| [10] |
D. Herzog, V. Seyda, E. Wycisk, C. Emmelmann, Acta Mater. 117, 371 (2016)
DOI URL |
| [11] | A. Saboori, A. Aversa, G. Marchese, S. Biamino, M. Lombardi, P. Fino, Appl. Sci. Basel 10, 3310 (2020) |
| [12] | L. Liu, Q. Ding, Y. Zhong, J. Zou, J. Wu, Y.L. Chiu, J. Li, Z. Zhang, Q. Yu, Z. Shen, Mater. Today 21, 354 (2018) |
| [13] |
Z.J. Sun, X.P. Tan, S.B. Tor, C.K. Chua, NPG Asia Mater. 10, 127 (2018)
DOI URL |
| [14] |
N. Yang, J. Yee, B. Zheng, K. Gaiser, T. Reynolds, L. Clemon, W.Y. Lu, J.M. Schoenung, E.J. Lavernia, J. Therm. Spray Technol. 26, 610 (2017)
DOI URL |
| [15] |
Z. Yan, K. Zou, M. Cheng, Z. Zhou, L. Song, J. Mater. Res. Technol. 15, 582 (2021)
DOI URL |
| [16] | A. Aversa, A. Saboori, E. Librera, M. de Chirico, S. Biamino, M.Lombardi, P. Fino, Addit. Manuf. 34(101274), 101274 (2020) |
| [17] | A. Saboori, A. Aversa, F. Bosio, E. Bassini, E. Librera, M. DeChirico, S. Biamino, D. Ugues, P. Fino, M. Lombardi, Mater. Sci.Eng. A 766, 138360 (2019) |
| [18] |
K. Zhang, S. Wang, W. Liu, X. Shang, Mater. Des. 55, 104 (2014)
DOI URL |
| [19] |
P. Guo, B. Zou, C. Huang, H. Gao, J. Mater. Process. Technol. 240, 12 (2017)
DOI URL |
| [20] | D. Gu, X. Shi, R. Poprawe, D.L. Bourell, R. Setchi, J. Zhu,Science 372, 932 (2021) |
| [21] | K. Mertová, J. Džugan, M. Roudnická, M. Daniel, D. Vojtěch, M. Seifi, J.J. Lewandowski,Metals 10, 1340 (2020) |
| [22] |
P. Wang, M.H. Goh, Q. Li, M.L.S. Nai, J. Wei, Virtual Phys. Prototy. 15, 251 (2020)
DOI URL |
| [23] |
B. Brown, W. Everhart, J. Dinardo, Rapid Prototyp. J. 22, 801(2016)
DOI URL |
| [24] | A.M. Roach, B.C. White, A. Garland, B.H. Jared, J.D. Carroll, B.L. Boyce, Addit. Manuf. 32, 101090 (2020) |
| [25] |
J. Dzugan, M. Seifi, R. Prochazka, M. Rund, P. Podany, P. Konopik, J.J. Lewandowski, Mater. Charact. 143, 94 (2018)
DOI URL |
| [26] |
D. Barba, C. Alabort, Y. Tang, M. Viscasillas, R. Reed, E. Alabort, Mater. Des. 186, 108235 (2020)
DOI URL |
| [27] | A. Saboori, G. Piscopo, M. Lai, A. Salmi, S. Biamino, Mater. Sci. Eng. A 780, 139179 (2020) |
| [28] |
J. Shi, P. Zhu, G. Fu, S. Shi, Opt. Laser. Technol. 101, 341 (2018)
DOI URL |
| [29] |
W. Yang, Y. Tarng, J. Mater. Process. Technol. 84, 122 (1998)
DOI URL |
| [30] |
M. Ma, Z. Wang, D. Wang, X. Zeng, Opt. Laser. Technol. 45, 209(2013)
DOI URL |
| [31] | H.Z. Jiang, Z.Y. Li, T. Feng, P.Y. Wu, Q.S. Chen, S.K. Yao, J.Y. Hou, Acta Metall. Sin. -Engl. Lett. 35, 773 (2021) |
| [32] | Z. Li, T. Voisin, J.T. McKeown, J.C. Ye, T. Braun, C. Kamath, W.E. King, Y.M. Wang, Int. J.Plasticity 120, 395 (2019) |
| [33] |
T. Debroy, H.L. Wei, J.S. Zuback, T. Mukherjee, J.W. Elmer, J.O. Milewski, A.M. Beese, A. Wilson-Heid, A. De, W. Zhang, Prog. Mater. Sci. 92, 112 (2018)
DOI URL |
| [34] |
J. Li, D. Deng, X. Hou, X. Wang, G. Ma, D. Wu, G. Zhang, Mater. Sci. Technol. 32, 1223 (2016)
DOI URL |
| [35] |
B. Barkia, P. Aubry, P. Haghi-Ashtiani, T. Auger, L. Gosmain, F. Schuster, H. Maskrot, J. Mater. Sci. Technol. 41, 209 (2020)
DOI |
| [36] | T. Kurzynowski, K. Gruber, W. Stopyra, B. Kuźnicka, E. Chlebus, Mater. Sci. Eng. A 718, 64 (2018) |
| [37] | A. Yadollahi, N. Shamsaei, S.M. Thompson, D.W. Seely, Mater. Sci. Eng. A 644, 171 (2015) |
| [38] | M. Shamsujjoha, S.R. Agnew, J.M. Fitz-Gerald, W.R. Moore, T.A. Newman, Metall. Mater. Trans. A 49, 3011 (2018) |
| [39] |
D. Kong, C. Dong, X. Ni, L. Zhang, J. Yao, C. Man, X. Cheng, K. Xiao, X. Li, J. Mater. Sci. Technol. 35, 1499 (2019)
DOI URL |
| [40] |
D. Kong, C. Dong, X. Ni, Z. Liang, C. Man, X. Li, Mater. Res. Lett. 8, 390 (2020)
DOI URL |
| [41] | M. Mukherjee,Materialia 7, 100359 (2019) |
| [42] |
C.-H. Shiau, M.D. McMurtrey, R.C. O’Brien, N.D. Jerred, R.D. Scott, J. Lu, X. Zhang, Y. Wang, L. Shao, C. Sun, Mater. Des. 204, 109644 (2021)
DOI URL |
| [43] | J.W. Elmer, S.M. Allen, T.W. Eagar, Metall. Mater. Trans. A 20, 2117 ( 1989) |
| [44] | I. Tolosa, F. Garciandía, F. Zubiri, F. Zapirain, A. Esnaola, Int. J. Adv. Manuf. Technol. 51, 639 (2010) |
| [45] |
I.A. Segura, L.E. Murr, C.A. Terrazas, D. Bermudez, J. Mireles, V.S.V. Injeti, K. Li, B. Yu, R.D.K. Misra, R.B. Wicker, J. Mater. Sci. Technol. 35, 351 (2019)
DOI |
| [46] | C. Elangeswaran, A. Cutolo, G.K. Muralidharan, C. de Formanoir, F. Berto, K. Vanmeensel, B. Van Hooreweder, Int. J.Fatigue 123, 31 (2019) |
| [47] | T.M. Mower, M.J. Long, Mater. Sci. Eng. A 651, 198 (2016) |
| [48] | J. R. Davis,Tensile testing, 2nd edn. (ASM International, United States of America, 2004), pp. 45-46. |
| [49] |
K. Saeidi, L. Kvetkova, F. Lofajc, Z.J. Shen, RSC Adv. 5, 20747 (2015)
DOI URL |
| [50] |
L. Cui, S. Jiang, J. Xu, R.L. Peng, R.T. Mousavian, J. Moverare, Mater. Des. 198, 109385 (2021)
DOI URL |
| [51] |
T. Voisin, J.B. Forien, A. Perron, S. Aubry, N. Bertin, A. Samanta, A. Baker, Y.M. Wang, Acta Mater. 203, 116476 (2021)
DOI URL |
| [52] |
X. Wu, Y. Zhu, Mater. Res. Lett. 5, 527 (2017)
DOI URL |
| [53] | X. Wu, M. Yang, F. Yuan, G. Wu, Y. Wei, X. Huang, Y. Zhu, P. Natl, Acad. Sci. USA 112, 14501 (2015) |
| [54] | J. He, Y. Ma, D. Yan, S. Jiao, F. Yuan, X. Wu, Mater. Sci. Eng. A 726, 288 (2018) |
| [55] |
Y. Zhu, X. Wu, Mater. Res. Lett. 7, 393 (2019)
DOI URL |
| [56] |
C. Sun, W. Chi, W. Wang, Y. Duan, Int. J. Mech. Sci. 205, 106591 (2021)
DOI URL |
| [1] | Shiqing Wang, Hao Cheng, Xiangru Li, Bo Song, Yusheng Shi. 4D printing of shape memory alloy metamaterials: Mechanisms, structures, and applications [J]. Metals Advances, 2026, 40(2): 8-25. |
| [2] | Qinyuan Zheng, Yi Lu, Chengwu Zheng, Peng Liu, Tian Liang, Yikun Luan, Dianzhong Li. Improving Ductility of a 3Mn Medium-Mn Steel by Manipulating the Austenite Reversion Path [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(9): 1583-1590. |
| [3] | Jiayu Wang, Ke Liu, Zhao Lei, Xing Li, Li Liu, Sujun Wu. Machine-Learning-Assisted Phase Prediction in High-Entropy Alloys Using Two-Step Feature Selection Strategy [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(8): 1261-1274. |
| [4] | Dongchao Li, Fen Zhang, Lanyue Cui, Yueling Guo, Rongchang Zeng. Accelerated Corrosion Rate of Wire Arc Additive Manufacturing of AZ91D Magnesium Alloy: The Formation of Nano-scaled AlMn Phase [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(7): 1069-1082. |
| [5] | Amir Behjat, Saber Sanaei, Mohammad Hossein Mosallanejad, Masoud Atapour, Abdollah Saboori. Electrochemical Behavior of Electron Beam Powder Bed Fused Ti536 Alloy under Simulated Inflammatory Conditions [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(6): 969-980. |
| [6] | Lingxiao Du, Hang Ding, Yun Xie, Li Ji, Wanbin Chen, Yunze Xu. Effect of Laser Energy Density on Microstructures and Properties of Additively Manufactured AlCoCrFeNi2.1 Eutectic High-Entropy Alloy [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(2): 233-244. |
| [7] | Yuheng Li, You Lv, Zehua Dong, Wei Guo, Xinxin Zhang, Xiaorong Zhou. Corrosion Behaviour of Wire Arc Additive Manufactured AA2024 Alloy Thin Wall Structure: The Influence of Interpass Rolling [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(12): 2197-2216. |
| [8] | Yi-Ming Chen, Jian-Lin Lu, Dong Yu, Hua-Yong Ren, Xiao-Bin Hu, Lei Wang, Zhi-Jun Wang, Jun-Jie Li, Jin-Cheng Wang. Accurate Identification of High Relative Density in Laser-Powder Bed Fusion Across Materials Using a Machine Learning Model with Dimensionless Parameters [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1645-1656. |
| [9] | Ali Kazemi Movahed, Reza Ghanavati, Abdollah Saboori, Luca Iuliano. A Review of Strategies for In Situ Mitigating of Residual Stress in Laser-Based Metal Additive Manufacturing: Insights, Innovations, and Challenges [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1657-1698. |
| [10] | Noa Lulu-Bitton, Nissim U. Navi, Noam Eliaz. Tensile Properties of Electrochemically Hydrogenated As-Built, Hot Isostatic Pressed and Heat-Treated Electron Beam Melted Ti-6Al-4V Alloys [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1711-1718. |
| [11] | Yuan Jiang, Baizhi Liang, Shewei Xin, Lei Shi, Siyuan Zhang, Kai Zhang, Hao Wang, Yi Yang, Lai-Chang Zhang. Cyclic Heat Treatment Induced Spheroidization of α Phase in Ti-5Al-3Mo-3V-2Cr-2Zr-1Nb-1Fe Alloy [J]. Acta Metallurgica Sinica (English Letters), 2025, 38(10): 1827-1838. |
| [12] | Erika Lannunziata, Mohammad Hossein Mosallanejad, Manuela Galati, Gabriele Piscopo, Abdollah Saboori. Analyzing the Interplay of Sintering Conditions on Microstructure and Hardness in Indirect Additive Manufacturing of 17-4PH Stainless Steel [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(9): 1611-1620. |
| [13] | Lan Zhang, Dao-Kui Xu, Bao-Jie Wang, Cui-Lan Lu, Shuo Wang, Xiang-Bo Xu, Dong-Liang Wang, Xin Lv, En-Hou Han. Mechanical Behavior and Failure Mechanism of an As-Extruded Mg-11wt%Y Alloy at Elevated Temperature [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(6): 969-981. |
| [14] | Jinpeng Hu, Tao Sun, Fujun Cao, Yifu Shen, Zhiyuan Yang, Chan Guo. Enhanced Strength-Ductility Synergy in Submerged Friction Stir Processing ER2319 Alloy Manufactured by Wire-Arc Additive Manufacturing via Creating Ultrafine Microstructure [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(5): 793-807. |
| [15] | Pengwei Jiang, Gang Wang, Yaosha Wu, Zhigang Zheng, Zhaoguo Qiu, Tongchun Kuang, Jibo Huang, Dechang Zeng. Microstructure Evolution, Tribological and Corrosion Properties of Amorphous Alloy Strengthening Stainless Steel Fabricated by Selective Laser Melting in NaCl Solution [J]. Acta Metallurgica Sinica (English Letters), 2024, 37(5): 825-839. |
| Viewed | ||||||
|
Full text |
|
|||||
|
Abstract |
|
|||||
WeChat
