Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (3): 375-388.DOI: 10.1007/s40195-021-01349-4
Special Issue: 2022年增材制造专辑; 铝及铝合金 2022
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Haoxiang Wang1,2, Xin Lin1,2(
), Nan Kang1,2(
), Zehao Qin1,2, Shuoqing Shi1,2, Jiacong Li1,2, Weidong Huang1,2
Received:2021-07-12
Revised:2021-09-04
Accepted:2021-09-28
Online:2022-02-01
Published:2022-02-01
Contact:
Xin Lin,Nan Kang
About author:Nan Kang, nan.kang@nwpu.edu.cnHaoxiang Wang, Xin Lin, Nan Kang, Zehao Qin, Shuoqing Shi, Jiacong Li, Weidong Huang. Interfacial Characteristics and Mechanical Behavior of Hybrid Manufactured AlSi10Mg-Al6061 Bimetal via Selective Laser Melting and Forging[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(3): 375-388.
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| Materials | Si | Mg | Mn | Fe | Zn | Cu | Al |
|---|---|---|---|---|---|---|---|
| AlSi10Mg powder | 9.67 | 0.41 | < 0.01 | 0.08 | < 0.01 | 0.01 | Bal. |
| Substrate Al6061 | 0.66 | 0.90 | 0.41 | 0.45 | 0.15 | 0.23 | Bal. |
Table 1 Chemical composition (wt.%) of the materials used in the current study
| Materials | Si | Mg | Mn | Fe | Zn | Cu | Al |
|---|---|---|---|---|---|---|---|
| AlSi10Mg powder | 9.67 | 0.41 | < 0.01 | 0.08 | < 0.01 | 0.01 | Bal. |
| Substrate Al6061 | 0.66 | 0.90 | 0.41 | 0.45 | 0.15 | 0.23 | Bal. |
| Process parameters | Value |
|---|---|
| Laser power (W) | 340 |
| Scanning speed (mm/s) | 1600 |
| The thickness of the first layer (μm) | 0/30 |
| The thickness of the subsequent layers (μm) | 30 |
| Hatch space (mm) | 0.1 |
| Scanning strategy | Strip type/interlayer angle 67 degree |
| Preheating temperature (°C) | 150 |
Table 2 SLM Process parameters
| Process parameters | Value |
|---|---|
| Laser power (W) | 340 |
| Scanning speed (mm/s) | 1600 |
| The thickness of the first layer (μm) | 0/30 |
| The thickness of the subsequent layers (μm) | 30 |
| Hatch space (mm) | 0.1 |
| Scanning strategy | Strip type/interlayer angle 67 degree |
| Preheating temperature (°C) | 150 |
| Procedure | 1 | 2 | 3 |
|---|---|---|---|
| Voltage (kV) | 4 | 6 | 4 |
| Milling angle (°) | 10.5 | 4.5 | 4.5 |
| Milling time (min) | 20 | 120 | 30 |
| Rotation speed (rpm) | 1.5 | 1.5 | 1.5 |
| Milling area (Φ, mm) | 10 | 10 | 10 |
Table 3 Ar-ion milling parameters
| Procedure | 1 | 2 | 3 |
|---|---|---|---|
| Voltage (kV) | 4 | 6 | 4 |
| Milling angle (°) | 10.5 | 4.5 | 4.5 |
| Milling time (min) | 20 | 120 | 30 |
| Rotation speed (rpm) | 1.5 | 1.5 | 1.5 |
| Milling area (Φ, mm) | 10 | 10 | 10 |
Fig. 2 Schematic diagram of a tensile specimens and b nanoindentation test positionwhere $A_{0}$ is the initial cross-sectional area of the tensile specimens of the hybrid parts, $\varepsilon_{i}$ is the local true strain obtained by the DIC approach, $A_{i}$ is the cross-sectional area of the tensile specimens corresponding to $\varepsilon_{i}$, and $F_{i}$ is the tensile force applied in tensile tests.
Fig. 6 a OM micrograph of the interfacial bonding zone of the hybrid part, b SEM microstructure of the interfacial bonding zone of the hybrid part, c enlarged image of area c (dilution zone) in Fig. 6b, d SEM microstructure of the melt pool of SLM-AlSi10Mg far away from the interface, e and f enlarged images of area e (the center of the melt pool), f (the boundary of the melt pool) in Fig. 6d
Fig. 7 EBSD IPF map of the interface of the hybrid part and EBSD pole figures of a columnar grains of SLM AlSi10Mg, b equiaxed grains of SLM AlSi10Mg, c first deposited layer, d substrate alloyFull size image
Fig. 9 Room-temperature tensile properties of the hybrid parts: a engineering stress-engineering strain curves and fracture positions (the red line in the inset indicating the position of the interface), b histogram of tensile properties
| Sample No. | 0 | 1 | 2 | 3 | 4 | 5 | 6 |
|---|---|---|---|---|---|---|---|
| YS (MPa) | 313 ± 3 | 272 ± 5 | 279 ± 4 | 272 ± 5 | 275 ± 3 | 272 ± 6 | 243 ± 6 |
| UTS (MPa) | 345 ± 3 | 334 ± 12 | 338 ± 1 | 337 ± 4 | 353 ± 5 | 362 ± 12 | 467 ± 12 |
| Elongation (%) | 9.5 ± 1.5 | 5.6 ± 1.9 | 4.1 ± 0.1 | 4.0 ± 0.9 | 4.4 ± 0.1 | 3.5 ± 0.8 | 8.6 ± 0.9 |
| YS (UTS) | 0.91 | 0.81 | 0.83 | 0.81 | 0.78 | 0.75 | 0.52 |
Table 4 Tensile properties of the hybrid parts (samples 1-5), the substrate Al6061 alloy (sample 0) and the SLM-AlSi10Mg (sample 6)
| Sample No. | 0 | 1 | 2 | 3 | 4 | 5 | 6 |
|---|---|---|---|---|---|---|---|
| YS (MPa) | 313 ± 3 | 272 ± 5 | 279 ± 4 | 272 ± 5 | 275 ± 3 | 272 ± 6 | 243 ± 6 |
| UTS (MPa) | 345 ± 3 | 334 ± 12 | 338 ± 1 | 337 ± 4 | 353 ± 5 | 362 ± 12 | 467 ± 12 |
| Elongation (%) | 9.5 ± 1.5 | 5.6 ± 1.9 | 4.1 ± 0.1 | 4.0 ± 0.9 | 4.4 ± 0.1 | 3.5 ± 0.8 | 8.6 ± 0.9 |
| YS (UTS) | 0.91 | 0.81 | 0.83 | 0.81 | 0.78 | 0.75 | 0.52 |
Fig. 10 SEM images of the fracture morphologies: a-c substrate Al6061 alloy, d-f hybrid part broken in the substrate area, g-i hybrid part broken in the interface area, j-l SLM-AlSi10Mg
Fig. 12 a-c True stress-true strain curves of different regions in sample 1, sample 3, and sample 5, respectively, d and e true stress-true strain curves and the corresponding strain hardening rate-true strain curves of the three groups of samples in the interface region and the substrate region, respectively
| Sample No. | Region | $K$ | $n$ | $\sigma_{\text{u}}$ |
|---|---|---|---|---|
| Sample 1 | SLM-part | 897.999 | 0.2472 | 635.678 |
| Interface | 500.121 | 0.11315 | 390.837 | |
| Substrate | 492.767 | 0.10625 | 383.819 | |
| Sample 3 | SLM-part | 987.888 | 0.25108 | 698.253 |
| Interface | 478.032 | 0.10169 | 378.885 | |
| Substrate | 491.099 | 0.09278 | 393.885 | |
| Sample 5 | SLM-part | 1025.965 | 0.29172 | 716.23 |
| Interface | 492.059 | 0.09924 | 391.245 | |
| Substrate | 497.579 | 0.0828 | 395.634 |
Table 5 Constitutive properties of various regions of the hybrid parts
| Sample No. | Region | $K$ | $n$ | $\sigma_{\text{u}}$ |
|---|---|---|---|---|
| Sample 1 | SLM-part | 897.999 | 0.2472 | 635.678 |
| Interface | 500.121 | 0.11315 | 390.837 | |
| Substrate | 492.767 | 0.10625 | 383.819 | |
| Sample 3 | SLM-part | 987.888 | 0.25108 | 698.253 |
| Interface | 478.032 | 0.10169 | 378.885 | |
| Substrate | 491.099 | 0.09278 | 393.885 | |
| Sample 5 | SLM-part | 1025.965 | 0.29172 | 716.23 |
| Interface | 492.059 | 0.09924 | 391.245 | |
| Substrate | 497.579 | 0.0828 | 395.634 |
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