The success in synthesizing high purity SnO2 nanobelts via self-propagating high temperature synthesis was achieved. According to the experimental results, a relationship between the residual heat of the reaction system at 2848 K and SnO2 nanobelts yield was identified. The most appropriate formula for this self-propagating high temperature synthesis method is turned out to be composed of Sn powder and thermite with weight ratio of 1:1.
LIU Nian
,
ZHANG Guo-Dong
. Optimal design of self-propagating high temperature one-dimensional nano-SnO2 synthesis[J]. Acta Metallurgica Sinica (English Letters), 2011
, 24(4)
: 321
-325
.
DOI: 10.11890/1006-7191-114-321
[1] O. Lupan, L. Chow, G. Chai, A. Schulte, S.Park and H. Heinrich, Mater Sci Eng B 157 (2009) 101.
[2] G. Cheng, K. Wu, P. Zhao, Y. Cheng, X. He and K. Huang, J Cryst Growth 309 (2007) 53.
[3] M. Li, Q. Lu, Y. Nuli and X. Qian, ElectrochemSolid-State Lett 10(8) (2007) K33.
[4] Z.Q. Liu, D.H. Zhang, S. Han, C. Li, T. Tang, W. Jin,X.L. Liu, B. Lei and C.W. Zhou, Adv Mater 15 (2003)1754.
[5] J.X. Wang, D.F. Liu, X.Q. Yan, H.J. Yuan, L.J. Ci, Z.P.Zhou, Y. Gao, L. Song, L.F. Liu, W.Y. Zhou, G. Wang and S.S. Xie, Solid State Commun 130 (2004) 89.
[6] Y.Q. Chen, X.F. Cui, K. Zhang, D.Y. Pan, S.Y. Zhang, B.Wang and J.G. Hou, Chem Phys Lett 369 (2003) 16.
[7] D. Calestani, M. Zha, A. Zappettini, L. Lazzarini, G.Salviati, L. Zanotti and G. Sberveglieri, Mater Sci Eng C 25 (2005) 625.