Acta Metallurgica Sinica (English Letters) ›› 2022, Vol. 35 ›› Issue (11): 1903-1911.DOI: 10.1007/s40195-022-01415-5
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Cunyun Hu1,2, Hefei Huang2,3(
), Zhenbo Zhu2,3, Awen Liu2,3, Yan Li1,2,3(
)
Received:2022-02-17
Revised:2022-03-04
Accepted:2022-03-17
Online:2022-11-10
Published:2022-05-19
Contact:
Hefei Huang, huanghefei@sinap.ac.cn; Yan Li, liyan@sinap.ac.cn
Cunyun Hu, Hefei Huang, Zhenbo Zhu, Awen Liu, Yan Li. Effect of Post-irradiation Annealing on Microstructure Evolution and Hardening in GH3535 Alloy Irradiated by Au Ions[J]. Acta Metallurgica Sinica (English Letters), 2022, 35(11): 1903-1911.
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| Ni | Mo | Cr | Fe | Mn | Si | Al, Cu, C |
|---|---|---|---|---|---|---|
| Bal | 16.50 | 6.96 | 4.20 | 0.71 | 0.46 | < 0.1 |
Table 1 Alloy composition of the GH3535 alloy (wt%)
| Ni | Mo | Cr | Fe | Mn | Si | Al, Cu, C |
|---|---|---|---|---|---|---|
| Bal | 16.50 | 6.96 | 4.20 | 0.71 | 0.46 | < 0.1 |
Fig. 1 Irradiation damage regions of the displacement per atom (dpa) and Au3+ concentration profiles produced by 6 MeV Au3+ with dose of 6.42 × 1014 ions/cm2
| Samples | Irradiation dose (ion/cm2) | Annealed temperature (℃) |
|---|---|---|
| Unirr | 0 | 0 |
| Irr | 6.42 × 1014 | RT |
| Irr. + An. 200 ℃ | 6.42 × 1014 | 200 |
| Irr. + An. 350 ℃ | 6.42 × 1014 | 350 |
| Irr. + An. 500 ℃ | 6.42 × 1014 | 500 |
| Irr. + An. 650 ℃ | 6.42 × 1014 | 650 |
| Irr. + An. 750 ℃ | 6.42 × 1014 | 750 |
| Irr. + An. 850 ℃ | 6.42 × 1014 | 850 |
Table 2 Specific parameters of the annealing experiment
| Samples | Irradiation dose (ion/cm2) | Annealed temperature (℃) |
|---|---|---|
| Unirr | 0 | 0 |
| Irr | 6.42 × 1014 | RT |
| Irr. + An. 200 ℃ | 6.42 × 1014 | 200 |
| Irr. + An. 350 ℃ | 6.42 × 1014 | 350 |
| Irr. + An. 500 ℃ | 6.42 × 1014 | 500 |
| Irr. + An. 650 ℃ | 6.42 × 1014 | 650 |
| Irr. + An. 750 ℃ | 6.42 × 1014 | 750 |
| Irr. + An. 850 ℃ | 6.42 × 1014 | 850 |
Fig. 4 Enlarged BF TEM images and corresponding DF TEM images at their peak damage regions showing the characteristics of dislocation loops: a sample before annealing; b-e samples after annealing at 200, 350, 500, 650 °C
Fig. 7 a Size distribution of dislocation loops at peak damage regions in the irradiated samples before and after annealing. b Mean size and number density of dislocation loops at the peak damage regions in the irradiated samples before and after annealing
| Sample | H0 (GPa) | ΔH0 (GPa) |
|---|---|---|
| Unirr | 3.02 ± 0.15 | |
| Unan | 5.11 ± 0.13 | 2.09 ± 0.02 |
| Irr. + An. 200 °C | 4.89 ± 0.13 | 1.87 ± 0.03 |
| Irr. + An. 350 °C | 4.92 ± 0.23 | 1.90 ± 0.08 |
| Irr. + An. 500 °C | 4.58 ± 0.22 | 1.56 ± 0.07 |
| Irr. + An. 650 °C | 4.22 ± 0.22 | 1.20 ± 0.07 |
| Irr. + An. 750 °C | 5.69 ± 0.20 | 2.67 ± 0.05 |
| Irr. + An. 850 °C | 4.32 ± 0.14 | 1.30 ± 0.02 |
Table 3 Nanohardness (H0) and its increment (ΔH0) for the investigated samples
| Sample | H0 (GPa) | ΔH0 (GPa) |
|---|---|---|
| Unirr | 3.02 ± 0.15 | |
| Unan | 5.11 ± 0.13 | 2.09 ± 0.02 |
| Irr. + An. 200 °C | 4.89 ± 0.13 | 1.87 ± 0.03 |
| Irr. + An. 350 °C | 4.92 ± 0.23 | 1.90 ± 0.08 |
| Irr. + An. 500 °C | 4.58 ± 0.22 | 1.56 ± 0.07 |
| Irr. + An. 650 °C | 4.22 ± 0.22 | 1.20 ± 0.07 |
| Irr. + An. 750 °C | 5.69 ± 0.20 | 2.67 ± 0.05 |
| Irr. + An. 850 °C | 4.32 ± 0.14 | 1.30 ± 0.02 |
| Sample | M | b (nm) | $\mu$(GPa) | ɑ | Number density (× 1023 m-3) | Mean size (nm) | σ (GPa) |
|---|---|---|---|---|---|---|---|
| Irr. + Unan | 3.06 | 0.254 | 83.20 | 0.33 | 1.62 | 3.69 | 0.52 |
| Irr. + An. 200 °C | 1.30 | 3.60 | 0.46 | ||||
| Irr. + An. 350 °C | 7.89 | 4.21 | 0.39 | ||||
| Irr. + An. 500 °C | 4.05 | 4.02 | 0.27 | ||||
| Irr. + An. 650 °C | 0.13 | 6.21 | 0.19 |
Table 4 Parameters related to the dislocation loops and calculated yield stress
| Sample | M | b (nm) | $\mu$(GPa) | ɑ | Number density (× 1023 m-3) | Mean size (nm) | σ (GPa) |
|---|---|---|---|---|---|---|---|
| Irr. + Unan | 3.06 | 0.254 | 83.20 | 0.33 | 1.62 | 3.69 | 0.52 |
| Irr. + An. 200 °C | 1.30 | 3.60 | 0.46 | ||||
| Irr. + An. 350 °C | 7.89 | 4.21 | 0.39 | ||||
| Irr. + An. 500 °C | 4.05 | 4.02 | 0.27 | ||||
| Irr. + An. 650 °C | 0.13 | 6.21 | 0.19 |
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