Acta Metallurgica Sinica (English Letters) ›› 1998, Vol. 11 ›› Issue (4): 291-295.

• Research paper • Previous Articles     Next Articles

SYNTHESIS OF TiN BY MICROWAVE CARBOTHERMAL REDUCTION OF TiO_2

B.H Liu; Y Zhang; S.X. Ouyang; and H.C. Gu (Research Institute of Technical Chemical Physics, East China University of Science and Technology,Shanghai 200237, China)(Department of Materials Physics, University of Science and Technology Beijing, Beijing 100083, China)(State Key Laboratory for Synthesis and Processing of Advanced Materials, Wuhan University of Technology, Wuhan 430070, China)   

  • Received:1998-08-25 Revised:1998-08-25 Online:1998-08-25 Published:2009-10-10

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Abstract: Titanium nitride powder was synthesized by microwave carbothermal reduction of titanium oxide. The mechanism and thermal dynamics of the reaction process were studied. The results show that the microwave carbothermal reduction technology has unique advantages over the conventional reduction methods. It can not only lower the reaction temperature, shorten the synthesis cycle, but also refine the product particles,as well as improving the reactivity of the powder.

Key words: TiN microwave, carbothermal reduction

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